Reaction
ChemicalBook > CAS DataBase List > 5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine

5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine

Reaction
Product Name
5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine
CAS No.
942939-38-0
Chemical Name
5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine
Synonyms
f]azepine;Reaxys ID: 21143615;5-(11bS)-Dinaphtho[2;5-(11bS)-Dinaphtho[2,1-d;2]dioxaphosphepin-4-yl-5H-dibenz[b;3,4-a′]dinaphthalen-4-yl)-dibenzo[b,f]azepine;(S)-(+)-N-(3,5-Dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine;3,4-a'']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine;3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine,min.97%
CBNumber
CB82750837
Molecular Formula
C34H22NO2P
Formula Weight
507.53
MOL File
942939-38-0.mol
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5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine Property

Melting point:
246 °C
Boiling point:
711.5±63.0 °C(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-2.70±0.20(Predicted)
form 
solid
color 
yellow
Sensitive 
air sensitive, moisture sensitive
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Safety

WGK Germany 
3
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
744646
Product name
(S)-(+)-N-(3,5-Dioxa-4-phosphacyclohepta[2,1-a,3,4-a′]dinaphthalen-4-yl)-dibenzo[b,f]azepine
Purity
≥95% (elemental analysis)
Packaging
100mg
Price
$110
Updated
2024/03/01
Sigma-Aldrich
Product number
744646
Product name
(S)-(+)-N-(3,5-Dioxa-4-phosphacyclohepta[2,1-a,3,4-a′]dinaphthalen-4-yl)-dibenzo[b,f]azepine
Purity
≥95% (elemental analysis)
Packaging
500mg
Price
$350
Updated
2024/03/01
Strem Chemicals
Product number
15-1227
Product name
(S)-(+)-(3,5-Dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine, min. 97%
Packaging
100mg
Price
$90
Updated
2024/03/01
Strem Chemicals
Product number
15-1227
Product name
(S)-(+)-(3,5-Dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine, min. 97%
Packaging
500mg
Price
$354
Updated
2024/03/01
Ambeed
Product number
A857931
Product name
(S)-(3,5-Dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine
Purity
98%99%ee
Packaging
5g
Price
$990
Updated
2021/12/16
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5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine Chemical Properties,Usage,Production

Reaction

  1. The ligand is used in the stereodivergent α-allylation of linear aldehydes with dual iridium and amine catalysis.
  2. The ligand used in the direct, enantioselective iridium-catalyzed amination and (thio-) etherification of racemic allylic alcohols.
  3. The ligand used in an asymmetric, rhodium-catalyzed, intramolecular hydroacylation reaction. 

Uses

Phosphorous precursor for ligand synthesis

5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine Suppliers

Aladdin Scientific
Tel
+1-+1(833)-552-7181
Email
sales@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Strem Chemicals, Inc.
Tel
--
Fax
--
Email
info@strem.com
Country
United States
ProdList
4910
Advantage
86
Riedel-de Haen AG
Tel
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Fax
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Country
United States
ProdList
6773
Advantage
87

942939-38-0, 5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepineRelated Search:


  • Reaxys ID: 21143615
  • (S)-(+)-N-(3,5-Dioxa-4-phosphacyclohepta[2,1-a
  • 3,4-a']dinaphthalen-4-yl)-dibenzo[b,f]azepine >=95% (elemental analysis)
  • 3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine
  • 3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine, min. 97%
  • (S)-(+)-(3,5-DIOXA-4-PHOSPHACYCLOHEPTA[2,1-A;3,4-A']DINAPHTHALEN-4-YL)-5H-DIBENZ[B,F]AZEPINE,MIN.97%
  • 3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine,min.97%
  • (S)-(+)-(3,5-Dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine, min. 97%
  • 3,4-a′]dinaphthalen-4-yl)-dibenzo[b,f]azepine
  • 1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine
  • 5-(11bS)-Dinaphtho[2,1-d
  • (S)-(+)-N-(3,5-Dioxa-4-phosphacyclohepta[2,1-a,3,4-a′]dinaphthalen-4-yl)-dibenzo[b,f]azepine
  • 5-(11bS)-Dinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine
  • 5-(11bS)-5H-Dibenz[b,f]azepine-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl
  • 5H-Dibenz[b,f]azepine, 5-(11bS)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl-
  • 2]dioxaphosphepin-4-yl-5H-dibenz[b
  • 5-(11bS)-Dinaphtho[2
  • f]azepine
  • 5-((11bS)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)-5H-dibenzo[b,f]azepine
  • 3,4-a'']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine
  • 5-(11bS)-Dinaphtho[2,1-d:1’,2’-f][1,3,2]dioxaphosphepin-4-yl-5H-dibenz[b,f]azepine
  • 5-(11bS)-5H-Dibenz[b,f]azepine-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl
  • 942939-38-0
  • C34H22NO2P
  • Chiral Phosphine
  • CPN