2-Nitro-5-phenoxyaniline
- Product Name
- 2-Nitro-5-phenoxyaniline
- CAS No.
- 1552-17-6
- Chemical Name
- 2-Nitro-5-phenoxyaniline
- Synonyms
- (2-Nitro-6-phenoxyphenyl)amine;Benzenamine, 2-nitro-5-phenoxy-
- CBNumber
- CB83052550
- Molecular Formula
- C12H10N2O3
- Formula Weight
- 230.22
- MOL File
- 1552-17-6.mol
2-Nitro-5-phenoxyaniline Property
- Melting point:
- 148-150 °C
- Boiling point:
- 377.7±22.0 °C(Predicted)
- Density
- 1.322±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- -1.05±0.25(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CS-0100531
- Product name
- 2-Nitro-5-phenoxyaniline
- Purity
- >97.0%
- Packaging
- 250mg
- Price
- $30
- Updated
- 2021/12/16
- Product number
- CS-0100531
- Product name
- 2-Nitro-5-phenoxyaniline
- Purity
- >97.0%
- Packaging
- 1g
- Price
- $119
- Updated
- 2021/12/16
- Product number
- 015692
- Product name
- 2-Nitro-5-phenoxy-phenylamine
- Packaging
- 1g
- Price
- $185
- Updated
- 2021/12/16
- Product number
- 180257
- Product name
- (2-Nitro-6-phenoxyphenyl)amine
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- 180257
- Product name
- (2-Nitro-6-phenoxyphenyl)amine
- Packaging
- 1g
- Price
- $300
- Updated
- 2021/12/16
2-Nitro-5-phenoxyaniline Chemical Properties,Usage,Production
Synthesis
1635-61-6
108-95-2
1552-17-6
General steps: 1. Dissolve 2-nitro-5-chloroaniline (6 mmol), phenol (6 mmol) and potassium carbonate (9 mmol or 18 mmol, as appropriate) in dimethylsulfoxide (25 mL) and stir the reaction at 80 °C. The reaction time varied depending on the product: 5a required 5 h, 5b and 5d required 4 h, 5c required 4.35 h, and 5f required 8 h. The reaction was carried out at 80 °C. The reaction time varied depending on the product. After completion of the reaction, the mixture was cooled, poured into water, the precipitate was collected by filtration, dried and recrystallized from alcohol to give the target product 2-nitro-5-phenoxyaniline. 2. Alternative method: 2-nitro-5-chloroaniline (6 mmol), phenol (6 mmol) or the corresponding phenol (3 mmol) and potassium carbonate (9 mmol or 18 mmol, as appropriate) are dissolved in dimethylsulfoxide (25 mL) and subjected to sonication at 80°C. The reaction time varies depending on the product. The reaction time varied depending on the product: 1 h for 3a, b and 5a-d, 6 h for 5e and 2 h for 3c and 5f. After completion of the reaction, the mixture was cooled, poured into water, the precipitate was collected by filtration, dried and recrystallized from alcohol to give the target product 2-nitro-5-phenoxyaniline.
References
[1] Russian Chemical Bulletin, 2015, vol. 64, # 8, p. 1971 - 1974
[2] Izv. Akad. Nauk, Ser. Khim., 2015, # 8, p. 1971 - 1974,4
[3] Journal of Heterocyclic Chemistry, 1997, vol. 34, # 3, p. 745 - 748
[4] Patent: US5162318, 1992, A
[5] Patent: US4034107, 1977, A
2-Nitro-5-phenoxyaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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