1-pinacolato-2-(1,8)diamo-naphthalenylborane

Product Name: 1-pinacolato-2-(1,8)diamo-naphthalenylborane
CAS No.: 1214264-88-6
Chemical Name: 1-pinacolato-2-(1,8)diamo-naphthalenylborane
Synonyms: (Pin)B-B(Dan);2-(4,4,5,5-Tetra;1-Phenaol-2- (1,8) Diaminonaphthylborane;1-pinacolato-2-(1,8)diamo-naphthalenylborane;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-...;1H-Naphtho[1,8-de][1,3,2]diazaborinine-2(3H)-boronic Acid Pinacol Ester;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-naphtho[1,8-de][1,3,2]diazaborinane;3-(Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,4-diaza-3-boratricyclo-[7.3.1.0^{5,13}]trideca-1(13);1H-Naphtho[1,8-de]-1,3,2-diazaborine, 2,3-dihydro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
CBNumber: CB83122626
Molecular Formula: C16H20B2N2O2
Formula Weight: 293.96
MOL File: 1214264-88-6.mol

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1-pinacolato-2-(1,8)diamo-naphthalenylborane Property

Melting point:: 186.7-187.4 °C
Boiling point:: 384.1±25.0 °C(Predicted)
Density: 1.14±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: -0.85±0.20(Predicted)
color: Off-white

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Safety

HS Code: 2934999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P302+P350IF ON SKIN: Gently wash with plenty of soap and water.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

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N-Bromosuccinimide Price

TRC

Product number: T889643
Product name: 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
Packaging: 500mg
Price: $130
Updated: 2021/12/16

AK Scientific

Product number: AMTB863
Product name: 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
Packaging: 250mg
Price: $23
Updated: 2021/12/16

AK Scientific

Product number: 8775DF
Product name: 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
Packaging: 1g
Price: $111
Updated: 2021/12/16

Matrix Scientific

Product number: 102827
Product name: 3-(Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,4-diaza-3-boratricyclo-[7.3.1.0{5,13}]trideca-1(13),5,7,9,11- pentaene
Purity: >95%
Packaging: 500mg
Price: $123
Updated: 2021/12/16

Apolloscientific

Product number: OR310571
Product name: 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
Packaging: 1g
Price: $125
Updated: 2021/12/16

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1-pinacolato-2-(1,8)diamo-naphthalenylborane Chemical Properties,Usage,Production

Synthesis

479-27-6

73183-34-3

1214264-88-6

General Steps: EXAMPLE: A 50 mL reaction flask was placed on a magnetic stirrer and pinacol ester of bisboronic acid (1.0 mmol, 1.0 eq.), 1,8-diaminonaphthalene (1.0 mmol, 1.0 eq.), and sodium methanol (1.0 mmol, 1.0 eq.) were added sequentially. After purging the reaction system with nitrogen three times under nitrogen protection, 10 mL of methanol was added as solvent. The reaction mixture was heated to 70 °C and stirred continuously for 4 hours. After completion of the reaction, the solvent methanol was removed by rotary evaporator. The crude product was purified by column chromatography to afford the target product 1-pinacol-2-(1,8)naphthalenediamine biboronate in 90% yield.

References

[1] Patent: CN106946916, 2017, A. Location in patent: Paragraph 0012
[2] Chemical Communications, 2014, vol. 50, # 61, p. 8299 - 8302

1-pinacolato-2-(1,8)diamo-naphthalenylborane Preparation Products And Raw materials

Raw materials

Preparation Products

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1-pinacolato-2-(1,8)diamo-naphthalenylborane Suppliers

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View Lastest Price from 1-pinacolato-2-(1,8)diamo-naphthalenylborane manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 1-pinacolato-2-(1,8)diamo-naphthalenylborane 1214264-88-6
Price: US $3.00-9.00/KG
Min. Order: 0.1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2025-07-02

Career Henan Chemical Co

Product: 1-pinacolato-2-(1,8)diamo-naphthalenylborane 1214264-88-6
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-01-08

1214264-88-6, 1-pinacolato-2-(1,8)diamo-naphthalenylboraneRelated Search:

1-pinacolato-2-(1,8)diamo-naphthalenylborane

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

3-(Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,4-diaza-3-boratricyclo-[7.3.1.0^{5,13}]trideca-1(13)

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-naphtho[1,8-de][1,3,2]diazaborinane

(Pin)B-B(Dan)

2-(4,4,5,5-Tetra

1H-Naphtho[1,8-de][1,3,2]diazaborinine-2(3H)-boronic Acid Pinacol Ester

1H-Naphtho[1,8-de]-1,3,2-diazaborine, 2,3-dihydro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-...

3-(Tetramethyl-1,3,2-dioxaborolan-2-yl)-2,4-diaza-3-boratricyclo-[7.3.1.0 {5,13}]trideca-1(13),5,7,9,11- pentaene

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,4-diaza-3-boratricyclo[7.3.1.0?13]trideca-1(13),5,7,9,11-pentaene

1-Phenaol-2- (1,8) Diaminonaphthylborane

1214264-88-6

C16H20B2N2O2