3-Chloro-4-fluoro-5-nitro-benzoic acid
- Product Name
- 3-Chloro-4-fluoro-5-nitro-benzoic acid
- CAS No.
- 132992-43-9
- Chemical Name
- 3-Chloro-4-fluoro-5-nitro-benzoic acid
- Synonyms
- 3-Chloro-4-fluoro-5-nitro-benzoic acid;Benzoic acid, 3-chloro-4-fluoro-5-nitro-;1,3,5-Triazine,2,4-dichloro-6-(5-pyrenyl)-
- CBNumber
- CB83361609
- Molecular Formula
- C7H3ClFNO4
- Formula Weight
- 219.55
- MOL File
- 132992-43-9.mol
3-Chloro-4-fluoro-5-nitro-benzoic acid Property
- Boiling point:
- 369.0±42.0 °C(Predicted)
- Density
- 1.689±0.06 g/cm3(Predicted)
- pka
- 3.17±0.10(Predicted)
- InChI
- InChI=1S/C7H3ClFNO4/c8-4-1-3(7(11)12)2-5(6(4)9)10(13)14/h1-2H,(H,11,12)
- InChIKey
- FSXCNZDIJKLGGU-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=CC([N+]([O-])=O)=C(F)C(Cl)=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C384098
- Product name
- 3-Chloro-4-fluoro-5-nitrobenzoicAcid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C384098
- Product name
- 3-Chloro-4-fluoro-5-nitrobenzoicAcid
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 9913DT
- Product name
- 3-Chloro-4-fluoro-5-nitrobenzoicacid
- Packaging
- 250mg
- Price
- $134
- Updated
- 2021/12/16
- Product number
- CD12153491
- Product name
- 3-Chloro-4-fluoro-5-nitrobenzoicacid
- Purity
- 95%
- Packaging
- 5g
- Price
- $330
- Updated
- 2021/12/16
- Product number
- BB20-3423
- Product name
- 3-Chloro-4-fluoro-5-nitro-benzoicacid
- Purity
- ＞95%
- Packaging
- 10g
- Price
- $720
- Updated
- 2021/12/16
3-Chloro-4-fluoro-5-nitro-benzoic acid Chemical Properties,Usage,Production
Synthesis
A round bottom flask was charged with 3-chloro-4-fluorobenzoic acid (2.50 g, 14.32 mmol) and sulfuric acid (10 ml), and nitric acid (0.91 mL, 21.48 mmol) was added slowly. The reaction mixture was stirred at rt for 30 min and then heated to 100 °C and stirred at that temperature for 2h. After cooling to room temperature, the reaction mixture was poured into ice cold water and the precipitated solids were collected by filtration and washed with water and dried to afford 3-Chloro-4-fluoro-5-nitro-benzoic acid (2.44 g, 78%).