5,6-Methylenedioxyindole

Product Name: 5,6-Methylenedioxyindole
CAS No.: 267-48-1
Chemical Name: 5,6-Methylenedioxyindole
Synonyms: 5,6-METHYLENEDIOXYINDOLE;5h-1,3-dioxolo(4,5-f)indole;5H-[1,3]dioxolo[4,5-f]indol;5-6-methylenedioxyindole tan crystals;5H-[1,3]Dioxolo[4,5-f]indole - [D71752]
CBNumber: CB8359278
Molecular Formula: C9H7NO2
Formula Weight: 161.16
MOL File: 267-48-1.mol

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5,6-Methylenedioxyindole Property

Melting point:: 110 °C
Boiling point:: 334.7±11.0 °C(Predicted)
Density: 1.425±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 16.93±0.20(Predicted)
color: tan

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Safety

Risk Statements: 20/21/22
Safety Statements: 36
WGK Germany: 3
RTECS: JI4650000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Precautionary statements: P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M220480
Product name: 5,6-Methylenedioxyindole
Packaging: 50mg
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: 2864AL
Product name: 5,6-Methylenedioxyindole
Packaging: 100mg
Price: $236
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0150936
Product name: 5,6-METHYLENEDIOXYINDOLE
Purity: 95.00%
Packaging: 5MG
Price: $501.58
Updated: 2021/12/16

Crysdot

Product number: CD11156064
Product name: 5H-[1,3]Dioxolo[4,5-f]indole
Purity: 97%
Packaging: 1g
Price: $545
Updated: 2021/12/16

Alichem

Product number: 267481
Product name: 5H-[1,3]Dioxolo[4,5-f]indole
Packaging: 1g
Price: $594
Updated: 2021/12/16

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5,6-Methylenedioxyindole Chemical Properties,Usage,Production

Uses

5H-[1,3]dioxolo[4,5-f]indole (5,6-Methylenedioxyindole) is an indole analogue commonly used in the preparation of other biologically active molecules, such as fungicides and anticancer agents.

Synthesis

86302-43-4

712-97-0

267-48-1

The general procedure for the synthesis of 5,6-methylenedioxyindole from [2-(1,1-dimethylethoxy)-2-oxoethyl]triphenylphosphonium inner salt and 6-nitropiperonyl aldehyde was as follows: In a 50 mL round-bottomed flask equipped with a magnetic stirrer, 6-nitropiperonyl aldehyde (2 mmol), [2-(1,1-dimethylethoxy)-2-oxoethyl]triphenylphosphonium inner salt (2.2 mmol), triphenylphosphine (4.6 mmol), and diphenyl ether (10 mL) were added in sequence. mmol), triphenylphosphine (4.6 mmol) and diphenyl ether (10 mL). The reaction mixture was heated to 260 °C and kept for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and the crude product was directly sampled onto a silica gel column. Separation was carried out by column chromatography using a gradient elution system of petroleum ether to 3:1 (v/v) petroleum ether/ethyl acetate to purify the target product 5,6-methylenedioxyindole.

References

[1] Tetrahedron Letters, 2018, vol. 59, # 19, p. 1851 - 1854

5,6-Methylenedioxyindole Preparation Products And Raw materials

Raw materials

Preparation Products

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5,6-Methylenedioxyindole Suppliers

China 61 India 2 Japan 1 Switzerland 1 United Kingdom 4 United States 9 Global 78

Shanghai Hanhong Scientific Co.,Ltd.

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Biokitchen

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Aikon International Limited

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Shanghai ZiHao Pharmaceutical Co., Ltd.

Tel: 021-13482410-12 13482410112
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Country: China
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View Lastest Price from 5,6-Methylenedioxyindole manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 5,6-METHYLENEDIOXYINDOLE 267-48-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1000KG
Release date: 2024-11-10

Career Henan Chemical Co

Product: 5,6-METHYLENEDIOXYINDOLE 267-48-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-09

267-48-1, 5,6-MethylenedioxyindoleRelated Search:

4,5-METHYLENEDIOXYINDOLE 2-methyl-3-(gamma-aminopropyl)-5,6-methylenedioxyindole 7-[2-[4-(2-Methoxyphenyl)-1-piperazinyl]ethyl]-5H-1,3-dioxolo[4, 5-f]i ndole tartrate 5,6-METHYLENEDIOXY-2-PHENYLINDOLE 5,6-METHYLENEDIOXYINDOLE-3-CARBOXYLIC ACID Solypertine 2-ETHYL-5,6-METHYLENDIOXYINDOLE 5-BENZYL-5H-[1,3]DIOXOLO[4,5-F]INDOLE-6-CARBOXYLIC ACID 5H-[1,3]DIOXOLO[4,5-F]INDOLE-6-CARBOXYLIC ACID METHYL ESTER 1-((1,1-Dimethyl)amino)-3-(5H-1,3-dioxolo(4,5-f)pyrido(3,4-b)indol-9-y loxy)-2-propanol 5,6-METHYLENEDIOXYINDOLE

5h-1,3-dioxolo(4,5-f)indole

5,6-METHYLENEDIOXYINDOLE

5-6-methylenedioxyindole tan crystals

5H-[1,3]dioxolo[4,5-f]indol

5H-[1,3]Dioxolo[4,5-f]indole - [D71752]

267-48-1

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Heterocyclic Building Blocks

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