(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL

Product Name: (5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL
CAS No.: 63870-39-3
Chemical Name: (5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL
Synonyms: NSC513582;ZERO/004602;ZINC02415220;ASINEX-REAG BAS 03825303;(3-Amino-1H-1,2,4-triazol-5-yl);(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL;(5-amino-2H-1,2,4-triazol-3-yl)methanol;methanol compound with 2-hydroxyacetic acid;(3-AMINO-1H-1,2,4-TRIAZOL-5-YL)METHANOL 2-HYDROXYACETIC ACID;(3-AMino-1H-1,2,4-triazol-5-yl)Methanol coMpound with 2-hydroxyacetic acid
CBNumber: CB8406064
Molecular Formula: C3H6N4O
Formula Weight: 114.11
MOL File: 63870-39-3.mol

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(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL Property

Melting point:: 114-115 °C(Solv: ethanol (64-17-5))
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
EPA Substance Registry System: Acetic acid, hydroxy-, compd. with 5-amino-1H-1,2,4-triazole-3-methanol (1:1) (63870-39-3)

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Safety

Hazard Codes: Xi
TSCA: TSCA listed

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Activate Scientific

Product number: AS147544
Product name: (5-Amino-1H-1,2,4-triazol-3-yl)methanol
Purity: 95%
Packaging: 1g
Price: $272
Updated: 2021/12/16

Activate Scientific

Product number: AS147544
Product name: (5-Amino-1H-1,2,4-triazol-3-yl)methanol
Purity: 95%
Packaging: 5G
Price: $918
Updated: 2021/12/16

Abosyn

Product number: 61-11608
Product name: (3-Amino-1H-1,2,4-triazol-5-yl)methanolcompoundwith2-hydroxyaceticacid
Purity: 95-98%
Packaging: 1g
Price: $315
Updated: 2021/12/16

Crysdot

Product number: CD11082274
Product name: (3-Amino-1H-1,2,4-triazol-5-yl)methanolcompoundwith2-hydroxyaceticacid
Purity: 95+%
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Crysdot

Product number: CD11082274
Product name: (3-Amino-1H-1,2,4-triazol-5-yl)methanolcompoundwith2-hydroxyaceticacid
Purity: 95+%
Packaging: 250mg
Price: $104
Updated: 2021/12/16

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(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL Chemical Properties,Usage,Production

Synthesis

79-14-1

2582-30-1

63870-39-3

Aminoguanidine bicarbonate (23.5 g, 172 mmol) was added in batches to a mixture of ethanoic acid (26.2 g, 345 mmol) and water (10 mL) over a period of 0.1 hours. During the addition, the reaction mixture was gently heated to maintain the internal temperature at 25 °C. Subsequently, concentrated nitric acid (1.0 mL) was added slowly and dropwise to the reaction system, and then the reaction mixture was heated to an internal temperature of 104-108 °C over 22 hours. Upon completion of the reaction, the heating was stopped and the solution was allowed to cool naturally with stirring. The slurry cooled to 10 °C was continued to be stirred for 2 h. Subsequently, it was filtered and the filter cake was washed with ethanol (EtOH). The resulting solid was dried overnight under vacuum to afford the target product (5-amino-1H-1,2,4-triazol-3-yl) methanol ethanolate (Product 88a, 29.5 g, 85% yield). Mass spectrometry analysis: calculated value (M + H)+ = 115, measured value (M + H)+ = 115.

References

[1] Patent: WO2012/83105, 2012, A1. Location in patent: Page/Page column 101
[2] Patent: WO2007/23381, 2007, A1. Location in patent: Page/Page column 54-55
[3] Patent: WO2004/74270, 2004, A2. Location in patent: Page 300
[4] Patent: US2005/176701, 2005, A1. Location in patent: Page/Page column 144

(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL Suppliers

China 28 India 1 Russia 2 United States 3 Global 34

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63870-39-3, (5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOLRelated Search:

ASINEX-REAG BAS 03825303

(5-AMINO-1H-1,2,4-TRIAZOL-3-YL)METHANOL

(3-AMino-1H-1,2,4-triazol-5-yl)Methanol coMpound with 2-hydroxyacetic acid

(5-amino-2H-1,2,4-triazol-3-yl)methanol

Acetic acid, hydroxy-, compd. with 5-amino-1H-1,2,4-triazole-3-methanol (1:1)

NSC513582

ZERO/004602

ZINC02415220

(3-Amino-1H-1,2,4-triazol-5-yl)

methanol compound with 2-hydroxyacetic acid

(3-AMINO-1H-1,2,4-TRIAZOL-5-YL)METHANOL 2-HYDROXYACETIC ACID

63870-39-3

C3H6N4OC2H4O3