(3-BROMO-4-CHLORO-PHENYL)-METHANOL
- Product Name
- (3-BROMO-4-CHLORO-PHENYL)-METHANOL
- CAS No.
- 329218-12-4
- Chemical Name
- (3-BROMO-4-CHLORO-PHENYL)-METHANOL
- Synonyms
- (3-Bromo-4-chlorophenyl);3-Bromo-4-chlorobenzyl alcohol;3-Bromo-4-chlorobenzenemethanol;Benzenemethanol, 3-bromo-4-chloro-;3-Bromo-4-chlorobenzyl alcohol 97%;(3-BROMO-4-CHLORO-PHENYL)-METHANOL
- CBNumber
- CB8414432
- Molecular Formula
- C7H6BrClO
- Formula Weight
- 221.48
- MOL File
- Mol file
(3-BROMO-4-CHLORO-PHENYL)-METHANOL Property
- Boiling point:
- 307.0±27.0 °C(Predicted)
- Density
- 1.685
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.89±0.10(Predicted)
- form
- solid
- color
- Off White
Safety
- HS Code
- 2906290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B683848
- Product name
- 3-Bromo-4-chlorobenzylalcohol
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- OR322285
- Product name
- 3-Bromo-4-chlorobenzylalcohol
- Purity
- 97%
- Packaging
- 1g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- 2601-D-08
- Product name
- 3-Bromo-4-chlorobenzyl alcohol
- Purity
- 97%
- Packaging
- 5G
- Price
- $140
- Updated
- 2021/12/16
- Product number
- X8250
- Product name
- 3-Bromo-4-chlorobenzylalcohol
- Packaging
- 25g
- Price
- $191
- Updated
- 2021/12/16
- Product number
- X8250
- Product name
- 3-Bromo-4-chlorobenzylalcohol
- Packaging
- 5g
- Price
- $91
- Updated
- 2021/12/16
(3-BROMO-4-CHLORO-PHENYL)-METHANOL Chemical Properties,Usage,Production
Synthesis
42860-10-6
329218-12-4
General procedure for the synthesis of 3-bromo-4-chlorobenzyl alcohol from 3-bromo-4-chlorobenzoic acid: A. To a mixture of 3-bromo-4-chlorobenzoic acid (10.0 g, 42.5 mmol) in THF (50 mL) was slowly added 1.0 M borane-THF solution (55.3 mL, 55.3 mmol) under nitrogen protection and at 0 °C. The reaction mixture was stirred overnight at room temperature and then carefully poured into a mixture of NaHCO3/H2O/ice and extracted with EtOAc. The organic layer was washed with saturated aqueous NaCl, dried over MgSO4, filtered and concentrated under reduced pressure to afford the target product 3-bromo-4-chlorobenzyl alcohol (9.4 g, 100%) as a clear, colorless oil.1H NMR (300 MHz, CDCl3) δ 7.61 (s, 1H), 7.41 (d, J = 5.1 Hz, 1H), 7.21 (d, J = 5.1 Hz, 1H), 4.63 (s, 2H), 2.12 (br s, 1H).
References
[1] Patent: WO2011/79102, 2011, A1. Location in patent: Page/Page column 132
[2] Synlett, 2014, vol. 25, # 1, p. 123 - 127
[3] Patent: WO2013/142396, 2013, A1. Location in patent: Page/Page column 55
[4] Patent: US2006/154915, 2006, A1. Location in patent: Page/Page column 29
[5] Patent: WO2003/99776, 2003, A1. Location in patent: Page 63
(3-BROMO-4-CHLORO-PHENYL)-METHANOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (3-BROMO-4-CHLORO-PHENYL)-METHANOL manufacturers
- Product
- (3-bromo-4-chlorophenyl)methanol 329218-12-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- Min98% HPLC
- Supply Ability
- g/kg/ton
- Release date
- 2020-01-08