2-FLUORO-5-NITRO-3-PICOLINE
- Product Name
- 2-FLUORO-5-NITRO-3-PICOLINE
- CAS No.
- 19346-46-4
- Chemical Name
- 2-FLUORO-5-NITRO-3-PICOLINE
- Synonyms
- 2-FLUORO-5-NITRO-3-PICOLINE;2-Fluorol-5-nitro-3-picoline;2-FLUORO-3-METHYL-5-NITROPYRIDINE;Pyridine, 2-fluoro-3-methyl-5-nitro-;2-FLUORO-5-NITRO-3-PICOLINE ISO 9001:2015 REACH;2-FLUORO-5-NITRO-3-PICOLINE (2-FLUORO-3-METHYL-5-NITROPYRIDINE)
- CBNumber
- CB8417367
- Molecular Formula
- C6H5FN2O2
- Formula Weight
- 156.11
- MOL File
- 19346-46-4.mol
2-FLUORO-5-NITRO-3-PICOLINE Property
- Boiling point:
- 265.7±35.0 °C(Predicted)
- Density
- 1.357±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- -4.17±0.20(Predicted)
- CAS DataBase Reference
- 19346-46-4(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,C
- Risk Statements
- 36/37/38-34
- Safety Statements
- 26-36-45-36/37/39
- HazardClass
- IRRITANT, IRRITANT-HARMFUL
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H227Combustible liquid
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- F598040
- Product name
- 2-Fluoro-3-methyl-5-nitropyridine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 024661
- Product name
- 2-Fluoro-3-methyl-5-nitropyridine
- Purity
- 98%
- Packaging
- 1g
- Price
- $18
- Updated
- 2021/12/16
- Product number
- N395
- Product name
- 2-Fluoro-5-nitro-3-picoline
- Packaging
- 1g
- Price
- $78
- Updated
- 2021/12/16
- Product number
- 024661
- Product name
- 2-Fluoro-3-methyl-5-nitropyridine
- Purity
- 98%
- Packaging
- 5g
- Price
- $94
- Updated
- 2021/12/16
- Product number
- 024661
- Product name
- 2-Fluoro-3-methyl-5-nitropyridine
- Purity
- 98%
- Packaging
- 25g
- Price
- $329
- Updated
- 2021/12/16
2-FLUORO-5-NITRO-3-PICOLINE Chemical Properties,Usage,Production
Synthesis
22280-56-4
2751-90-8
19346-46-4
2-Chloro-3-methyl-5-nitropyridine (15 g, 86.9 mmol, purchased from Maybridge Chemical Co.), potassium fluoride (12 g, 258 mmol), and tetraphenylphosphonium bromide (20 g, 47.7 mmol, purchased from Aldrich) were mixed in 200 mL of acetonitrile and the reaction was heated to reflux for 4 days. After completion of the reaction, the reaction mixture was diluted with ether (500 mL) and filtered, and the filtrate was concentrated to obtain the crude product. The crude product was ground with hot hexane (4 x 200 mL), the hexane solutions were combined and concentrated to afford the target compound 2-fluoro-3-methyl-5-nitropyridine as a solid (8.4 g, 60% yield). The product was identified by 1H NMR (DMSO-d6, 300 MHz): δ 2.42 (s, 3H), 8.43 (m, 1H), 8.95 (dd, J = 1.6 Hz, 1H); mass spectrum (CI/NH3) m/z: 157 (M + H)+.
References
[1] Patent: US5733912, 1998, A
2-FLUORO-5-NITRO-3-PICOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
2-FLUORO-5-NITRO-3-PICOLINE Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 001-857-928-2050 or 1-888-588-9418
- Fax
- 001-617-206-9595
- sales@chemreagents.com
- Country
- United States
- ProdList
- 10186
- Advantage
- 62
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- +86(24) 31938773(O)
- Fax
- qq:174941352
- sales@co-chem.com
- Country
- China
- ProdList
- 225
- Advantage
- 62
- Tel
- 0571-82693216
- Fax
- +86-571-82880190
- info@yuhaochemical.com
- Country
- China
- ProdList
- 6387
- Advantage
- 52
- Tel
- +86-18068513926
- Fax
- 0086-519-85153711
- Country
- China
- ProdList
- 1277
- Advantage
- 55
- Tel
- 0512-56316828 4008675858
- Fax
- +86-512-56316826
- sales@amateksci.com
- Country
- China
- ProdList
- 9874
- Advantage
- 55
- Tel
- 021-61317773
- Fax
- 021-61486878
- sales@aspirebio.com
- Country
- China
- ProdList
- 2880
- Advantage
- 58
- Tel
- 400-8592883
- Fax
- 0731-82251112
- sales@huatengsci.com
- Country
- China
- ProdList
- 5872
- Advantage
- 58
View Lastest Price from 2-FLUORO-5-NITRO-3-PICOLINE manufacturers
- Product
- 2-FLUORO-5-NITRO-3-PICOLINE 19346-46-4
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-08
- Product
- 2-FLUORO-5-NITRO-3-PICOLINE 19346-46-4
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-30
- Product
- 2-FLUORO-5-NITRO-3-PICOLINE 19346-46-4
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-12-10