2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE
- Product Name
- 2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE
- CAS No.
- 168823-65-2
- Chemical Name
- 2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE
- Synonyms
- 2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE;Pyridine, 2-(3-bromo-4-methoxyphenyl)-;2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE, 95+%
- CBNumber
- CB8417817
- Molecular Formula
- C12H10BrNO
- Formula Weight
- 264.12
- MOL File
- 168823-65-2.mol
2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE Property
- storage temp.
- Inert atmosphere,Room Temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- Z4270
- Product name
- 2-(3-Bromo-4-methoxyphenyl)pyridine
- Packaging
- 1g
- Price
- $117
- Updated
- 2021/12/16
- Product number
- 126591
- Product name
- 2-(3-Bromo-4-methoxyphenyl)pyridine
- Purity
- >95%
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- Z4270
- Product name
- 2-(3-Bromo-4-methoxyphenyl)pyridine
- Packaging
- 10g
- Price
- $517
- Updated
- 2021/12/16
- Product number
- 126591
- Product name
- 2-(3-Bromo-4-methoxyphenyl)pyridine
- Purity
- >95%
- Packaging
- 5g
- Price
- $720
- Updated
- 2021/12/16
- Product number
- COR0001460
- Product name
- 2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $727.65
- Updated
- 2021/12/16
2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE Chemical Properties,Usage,Production
Synthesis
5957-90-4
168823-65-2
N-bromosuccinimide (II) (108 mg, 0.6 mmol) was dissolved in N,N-dimethylformamide (0.2 M, 1.5 mL) as 2-(4-methoxyphenyl)pyridine (Ib) (56 mg, 0.3 mmol). 5-Cyclooctadiene ruthenium dichloride (8 mg, 10 mol%) was added as a catalyst and the reaction mixture was stirred at 150 °C for 24 hours. After completion of the reaction, the mixture was extracted with ethyl acetate (20 mL) and the organic phase was washed with water (10 mL x 3). The organic phase was dried with anhydrous sodium sulfate, filtered and the solvent was removed by rotary evaporator. The crude product was purified by column chromatography to afford 2-(3-bromo-4-methoxyphenyl)pyridine (III-b) (72 mg, colorless oil) in 90% yield.
References
[1] Angewandte Chemie - International Edition, 2015, vol. 54, # 50, p. 15284 - 15288
[2] Angew. Chem., 2015, vol. 127, # 50, p. 15499 - 15503,5
[3] Patent: CN104356053, 2017, B. Location in patent: Paragraph 0036; 0038; 0039
2-(3-BROMO-4-METHOXYPHENYL)PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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