ChemicalBook > CAS DataBase List > 1-Methylpyrrolidine-2-methanol

1-Methylpyrrolidine-2-methanol

Product Name
1-Methylpyrrolidine-2-methanol
CAS No.
3554-65-2
Chemical Name
1-Methylpyrrolidine-2-methanol
Synonyms
Einecs 222-608-7;1-METHYL-2-PYRROLIDINEMETHANOL;1-Methylpyrrolidine-2-methanol;2-PyrrolidineMethanol,1-Methyl-;(1-METHYLPYRROLIDIN-2-YL)METHANOL;(1-methyl-2-pyrrolidinyl)methanol;[(2S)-1-methyl-2-pyrrolidinyl]methanol
CBNumber
CB8448141
Molecular Formula
C6H13NO
Formula Weight
115.17
MOL File
3554-65-2.mol
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1-Methylpyrrolidine-2-methanol Property

Boiling point:
67-68 °C(Press: 12 Torr)
Density 
0.973±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
form 
solid
pka
14.77±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
CAS DataBase Reference
3554-65-2(CAS DataBase Reference)
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Safety

Hazard Codes 
Xn
Risk Statements 
22
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

AK Scientific
Product number
R422
Product name
1-Methylpyrrolidine-2-methanol
Packaging
1g
Price
$13
Updated
2021/12/16
Matrix Scientific
Product number
065627
Product name
(1-Methylpyrrolidin-2-yl)methanol
Packaging
5g
Price
$29
Updated
2021/12/16
Matrix Scientific
Product number
065627
Product name
(1-Methylpyrrolidin-2-yl)methanol
Packaging
25g
Price
$89
Updated
2021/12/16
AK Scientific
Product number
J96213
Product name
1-Methylpyrrolidine-2-methanol
Packaging
25g
Price
$90
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0078581
Product name
1-METHYLPYRROLIDINE-2-METHANOL
Purity
95.00%
Packaging
1G
Price
$823.44
Updated
2021/12/16
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1-Methylpyrrolidine-2-methanol Chemical Properties,Usage,Production

Definition

ChEBI: 1-Methylpyrrolidine-2-methanol is a N-alkylpyrrolidine.

Synthesis

50-00-0

498-63-5

3554-65-2

a) A mixture of (RS)-pyrrolidin-2-ylmethanol (1.00 g, 9.90 mmol, 1.0 eq.), 35% aqueous formaldehyde (10 mL) and 10% (1-methylpyrrolidin-2-yl)methanol was reacted with Pd/C (200 mg) for 18 hours with stirring under hydrogen atmosphere. Upon completion of the reaction, the mixture was filtered through a pad of diatomaceous earth and the filtrate was concentrated under reduced pressure and subsequently purified by silica gel column chromatography (eluent: 20% methanol/chloroform) to give a colorless liquid product (650 mg, 56% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 3.65 (dd, J = 10.0, 3.6 Hz, 1H), 3.43 (dd, J = 10.8, 2.0 Hz, 1H), 3.10-3.05 (m, 1H), 2.40-2.35 (m, 1H), 2.33 (s, 3H), 2.32-2.25 (m , 1H), 1.93-1.68 (m, 4H); mass spectrum (APCI+): m/z 116 [M + H]+.

References

[1] Patent: WO2012/127212, 2012, A1. Location in patent: Page/Page column 101

1-Methylpyrrolidine-2-methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-Methylpyrrolidine-2-methanol manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
1-Methyl-2-pyrrolidineMethanol 3554-65-2
Price
US $1.00/Kg
Min. Order
1Kg
Purity
98%
Supply Ability
20T
Release date
2024-07-19
Career Henan Chemical Co
Product
1-Methylpyrrolidine-2-methanol 3554-65-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2020-01-08

3554-65-2, 1-Methylpyrrolidine-2-methanolRelated Search:


  • 1-Methylpyrrolidine-2-methanol
  • (1-methyl-2-pyrrolidinyl)methanol
  • 1-METHYL-2-PYRROLIDINEMETHANOL
  • (1-METHYLPYRROLIDIN-2-YL)METHANOL
  • Einecs 222-608-7
  • 2-PyrrolidineMethanol,1-Methyl-
  • [(2S)-1-methyl-2-pyrrolidinyl]methanol
  • 3554-65-2
  • Pyrrole&Pyrrolidine&Pyrroline