ChemicalBook > CAS DataBase List > 3'-BROMO-4'-HYDROXYACETOPHENONE

3'-BROMO-4'-HYDROXYACETOPHENONE

Product Name: 3'-BROMO-4'-HYDROXYACETOPHENONE
CAS No.: 1836-06-2
Chemical Name: 3'-BROMO-4'-HYDROXYACETOPHENONE
Synonyms: 4-Acetyl-2-bromophenol;2-Bromo-4-acetylphenol;3'-BROMO-4'-HYDROXYACETOPHENONE;1-(3-Bromo-4-hydroxyphenyl)ethanone;Ethanone, 1-(3-bromo-4-hydroxyphenyl)-;1-(3-bromo-4-hydroxyphenyl)ethan-1-one
CBNumber: CB8498863
Molecular Formula: C8H7BrO2
Formula Weight: 215.04
MOL File: 1836-06-2.mol

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3'-BROMO-4'-HYDROXYACETOPHENONE Property

Melting point:: 111.0 to 115.0 °C
Boiling point:: 315.9±27.0 °C(Predicted)
Density: 1.586±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: soluble in Methanol
form: powder to crystal
pka: 6.63±0.18(Predicted)
color: White to Light yellow to Light orange

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Safety

Hazard Codes: Xn
Risk Statements: 22-36/37/38
Safety Statements: 26-36
HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B5158
Product name: 3'-Bromo-4'-hydroxyacetophenone
Purity: >98.0%(GC)(T)
Packaging: 1g
Price: $359
Updated: 2025/07/31

TRC

Product number: B993405
Product name: 1-(3-Bromo-4-hydroxyphenyl)ethanone
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B993405
Product name: 1-(3-Bromo-4-hydroxyphenyl)ethanone
Packaging: 100mg
Price: $310
Updated: 2021/12/16

AK Scientific

Product number: X3577
Product name: 1-(3-Bromo-4-hydroxyphenyl)ethanone
Packaging: 250mg
Price: $39
Updated: 2021/12/16

AK Scientific

Product number: J97801
Product name: 1-(3-Bromo-4-hydroxyphenyl)ethanone
Packaging: 1g
Price: $63
Updated: 2021/12/16

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3'-BROMO-4'-HYDROXYACETOPHENONE Chemical Properties,Usage,Production

Preparation

Preparation by diazotization of 5-amino-3-bromo-2- hydroxyacetophenone, followed by hydrolysis of the obtained diazonium salt (50%).

Synthesis

95-56-7

75-36-5

1836-06-2

2-Bromophenol (1.16 mL, 10.0 mmol) was dissolved in carbon disulfide (10 mL) and stirred under cooling in an ice-salt bath. Subsequently, anhydrous aluminum chloride (2.7 g, 20.0 mmol) was added in batches, followed by slow dropwise addition of acetyl chloride (0.754 mL, 11.0 mmol). The reaction mixture was maintained under stirring conditions for 1 hour and then refluxed overnight. Upon completion of the reaction, the mixture was quenched by adding a mixture of 1 M hydrochloric acid and ice to the mixture. The mixture was extracted using dichloromethane (3 times) and after combining the organic phases, it was dried and concentrated with anhydrous sodium sulfate. The residue was purified by silica gel column chromatography (eluent: 20% ethyl acetate/hexane to 40% ethyl acetate/hexane gradient elution) to afford the target product 3-bromo-4-hydroxyacetophenone (2.28 g, 53% yield).

References

[1] Journal of Medicinal Chemistry, 1980, vol. 23, # 7, p. 738 - 744
[2] Patent: WO2004/62661, 2004, A1. Location in patent: Page/Page column 27

3'-BROMO-4'-HYDROXYACETOPHENONE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3'-BROMO-4'-HYDROXYACETOPHENONE manufacturers

Career Henan Chemical Co

Product: 3'-BROMO-4'-HYDROXYACETOPHENONE 1836-06-2
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

1836-06-2, 3'-BROMO-4'-HYDROXYACETOPHENONERelated Search:

4'-Hydroxyacetophenone

3'-BROMO-4'-HYDROXYACETOPHENONE

1-(3-Bromo-4-hydroxyphenyl)ethanone

2-Bromo-4-acetylphenol

4-Acetyl-2-bromophenol

1-(3-bromo-4-hydroxyphenyl)ethan-1-one

Ethanone, 1-(3-bromo-4-hydroxyphenyl)-

1836-06-2

1836-06-3