2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile
- Product Name
- 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile
- CAS No.
- 23051-44-7
- Chemical Name
- 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile
- Synonyms
- (3 5 5-TRIMETHYLCYCLOHEX-2-ENYLIDENE)MA&;3-dicyanomethylene-1,5,5-trimethylcyclohexene;2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile;(3,5,5-trimethyl-2-cyclohexen-1-ylidene)propanedinitrile;(3,5,5-trimethyl-2-cyclohexen-1-ylidene)-propanedinitril;2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)propanedinitrile;Propanedinitrile, 2-(3,5,5-trimethyl-2-cyclohexen-1-ylidene)-
- CBNumber
- CB8500142
- Molecular Formula
- C12H14N2
- Formula Weight
- 186.25
- MOL File
- 23051-44-7.mol
2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile Property
- Melting point:
- 73-77 °C (lit.)
- Boiling point:
- 175-176 °C(Press: 19 Torr)
- Density
- 1.007±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- color
- White to Light yellow powder to crystal
- EPA Substance Registry System
- Propanedinitrile, (3,5,5-trimethyl-2-cyclohexen-1-ylidene)- (23051-44-7)
N-Bromosuccinimide Price
- Product number
- 643769
- Product name
- (3,5,5-Trimethylcyclohex-2-enylidene)malononitrile
- Packaging
- 1g
- Price
- $78.1
- Updated
- 2022/05/15
- Product number
- B536895
- Product name
- 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)propanedinitrile
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- B536895
- Product name
- 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)propanedinitrile
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- AS145241
- Product name
- 2-(3,5,5-Trimethylcyclohex-2-en-1-ylidene)propanedinitrile
- Purity
- 95%
- Packaging
- 1g
- Price
- $159
- Updated
- 2021/12/16
2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile Chemical Properties,Usage,Production
Synthesis
In a 100?mL round bottom flask, isophorone 3.45 g (25 mmol) and malononitrile 1.65 g (25 mmol) were dissolved in anhydrous ethanol 50 mL. Then sodium acetate trihydrate (1g, 12.5mmol) was added. The mixture was heated to 80°C and stirred for about 12h. The reaction progress was monitored by TLC. Once the starting isophorone disappeared on TLC and the target spot formed regularly, the reaction mixture was cooled to room temperature. The solid sodium acetate trihydrate was removed by filtration. 25mL Ethanol was removed in a vacuum. The left mixture stood still at 27°C overnight. The crystals were collected by filtration and washed carefully with cooled anhydrous ethanol. 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile can be obtained by recrystallization one more time from ethanol.
Structure and conformation
2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile (C12H14N2), monoclinic, P21/c (no. 14), a = 10.16290(10)Å, b = 8.25800(10)Å, c = 13.4328(2), β = 95.910(1)°, V = 1121.36(2)Å3, Z = 4, R gt (F) = 0.0380, wR ref (F2) = 0.1126, T = 294 K.
2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile Preparation Products And Raw materials
Raw materials
Preparation Products
2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile Suppliers
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View Lastest Price from 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile manufacturers
- Product
- 2-(3,5,5-trimethylcyclohex-2-en-1-ylidene)malononitrile 23051-44-7
- Price
- US $3000.00-30000.00/kg
- Min. Order
- 100kg
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2023-04-23