2-IODOBENZYLAMINE
- Product Name
- 2-IODOBENZYLAMINE
- CAS No.
- 39959-51-8
- Chemical Name
- 2-IODOBENZYLAMINE
- Synonyms
- (2-Iodophenyl)MethanaMine;2-IODOBENZYLAMINE;RARECHEM AL BW 0704;2-Iodobenzenemethanamine;1-(2-iodophenyl)methanamine;BenzeneMethanaMine, 2-iodo-
- CBNumber
- CB8704618
- Molecular Formula
- C7H8IN
- Formula Weight
- 233.05
- MOL File
- 39959-51-8.mol
2-IODOBENZYLAMINE Property
- Melting point:
- 63-65 °C
- Boiling point:
- 270.0±15.0 °C(Predicted)
- Density
- 1.772±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 8.54±0.10(Predicted)
- Appearance
- Light yellow to brown Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 5274AB
- Product name
- 2-Iodo-benzylamine
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 5274AB
- Product name
- 2-Iodo-benzylamine
- Packaging
- 1g
- Price
- $291
- Updated
- 2021/12/16
- Product number
- 5274AB
- Product name
- 2-Iodo-benzylamine
- Packaging
- 5g
- Price
- $744
- Updated
- 2021/12/16
- Product number
- HCH0049289
- Product name
- 2-IODOBENZYL AMINE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
- Product number
- HCH0049289
- Product name
- 2-IODOBENZYL AMINE
- Purity
- 95.00%
- Packaging
- 10G
- Price
- $1334.03
- Updated
- 2021/12/16
2-IODOBENZYLAMINE Chemical Properties,Usage,Production
Synthesis
405198-82-5
39959-51-8
Triphenylphosphine (6.8 g, 25.7 mmol) was added to an anhydrous tetrahydrofuran (THF, 100 mL) solution of 1-azidomethyl-2-iodobenzene (6.1 g, 23.4 mmol) at 0 °C. The reaction mixture was slowly warmed to room temperature and stirred for 16 hours. After the reaction was completed, the reaction mixture was diluted with ammonium hydroxide (20 mL) and stirring was continued for 3 hours. Subsequently, the reaction mixture was treated with 2M sodium hydroxide solution (30 mL) and stirred for another 1 hour. The reaction mixture was acidified to pH 2 with 3M hydrochloric acid, then diluted with ether and the layers were separated. The aqueous layer was alkalized to pH 9 with 2M sodium hydroxide solution and subsequently extracted with dichloromethane (3 times). The organic phases were combined, dried with anhydrous sodium sulfate and concentrated under vacuum to give an oily residue. The residue was treated with ether and filtered. The filtrate was purified by silica gel column chromatography using 95:5 dichloromethane:methanol as eluent to give 5.4 g (80% yield) of 2-iodobenzylamine.
References
[1] Patent: US2006/25433, 2006, A1. Location in patent: Page/Page column 107
[2] Tetrahedron, 2001, vol. 57, # 48, p. 9697 - 9710
[3] Angewandte Chemie - International Edition, 2005, vol. 44, # 35, p. 5679 - 5682
[4] Patent: US2006/24834, 2006, A1. Location in patent: Page/Page column 5-6; Sheet 7
[5] Journal of Organic Chemistry, 2010, vol. 75, # 24, p. 8410 - 8415
2-IODOBENZYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-IODOBENZYLAMINE manufacturers
- Product
- 2-IODOBENZYLAMINE 39959-51-8
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02