2-AMINO-4-CHLORO-6-NITROTOLUENE
- Product Name
- 2-AMINO-4-CHLORO-6-NITROTOLUENE
- CAS No.
- 219312-44-4
- Chemical Name
- 2-AMINO-4-CHLORO-6-NITROTOLUENE
- Synonyms
- 2-AMINO-4-CHLORO-6-NITROTOLUENE;5-Chloro-2-Methyl-3-nitroaniline;2-amino-4-chloro-7-nitro-toluene;5-chloro-2-methyl-3-nitrobenzenamine;Benzenamine, 5-chloro-2-methyl-3-nitro-
- CBNumber
- CB8731818
- Molecular Formula
- C7H7ClN2O2
- Formula Weight
- 186.6
- MOL File
- 219312-44-4.mol
2-AMINO-4-CHLORO-6-NITROTOLUENE Property
- Boiling point:
- 333.4±37.0 °C(Predicted)
- Density
- 1.415±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 1.08±0.10(Predicted)
- Appearance
- Yellow to orange Solid
Safety
- HS Code
- 2921490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C994185
- Product name
- 5-Chloro-2-methyl-3-nitroaniline
- Packaging
- 1mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C994185
- Product name
- 5-Chloro-2-methyl-3-nitroaniline
- Packaging
- 2mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CS-0054218
- Product name
- 5-Chloro-2-methyl-3-nitroaniline
- Packaging
- 1g
- Price
- $144
- Updated
- 2021/12/16
- Product number
- CS-0054218
- Product name
- 5-Chloro-2-methyl-3-nitroaniline
- Packaging
- 250mg
- Price
- $54
- Updated
- 2021/12/16
- Product number
- 2903AL
- Product name
- 5-Chloro-2-methyl-3-nitroaniline
- Packaging
- 100mg
- Price
- $169
- Updated
- 2021/12/16
2-AMINO-4-CHLORO-6-NITROTOLUENE Chemical Properties,Usage,Production
Synthesis
35572-79-3
219312-44-4
4-Iodo-2,6-dinitrotoluene (5.9 g, 23.60 mmol) was used as raw material and dissolved in a solvent mixture of methanol (10 mL) and 1,4-dioxane (5 mL). Under ice bath cooling conditions, 10 N hydrochloric acid (12 mL) and iron powder (3.96 g, 70.80 mmol) were slowly added. The reaction mixture was stirred at 80 °C for 3 h. The progress of the reaction was monitored by thin layer chromatography (TLC) until complete conversion of the feedstock. Upon completion of the reaction, 3.55 g of the light yellow powdery product 2-amino-4-chloro-6-nitrotoluene was obtained in 68.4% yield.
References
[1] Patent: CN108689937, 2018, A. Location in patent: Paragraph 0069; 0070; 0073; 0074
[2] Patent: CN108689936, 2018, A. Location in patent: Paragraph 0070; 0072; 0076; 0077
[3] Patent: US2010/63066, 2010, A1. Location in patent: Page/Page column 36
[4] Journal of the Chemical Society, 1905, vol. 87, p. 1265
[5] Patent: US5952362, 1999, A
2-AMINO-4-CHLORO-6-NITROTOLUENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-AMINO-4-CHLORO-6-NITROTOLUENE manufacturers
- Product
- 5-Chloro-2-methyl-3-nitroaniline 219312-44-4
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2020-01-10