2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE
- Product Name
- 2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE
- CAS No.
- 201849-21-0
- Chemical Name
- 2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE
- Synonyms
- 4-BROMO-2-CHLORO-1-ISOPROPOXYBENZENE;2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE;4-bromo-2-chloro-1-propan-2-yloxybenzene;Benzene, 4-bromo-2-chloro-1-(1-methylethoxy)-
- CBNumber
- CB8733908
- Molecular Formula
- C9H10BrClO
- Formula Weight
- 249.53
- MOL File
- 201849-21-0.mol
2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE Property
- Boiling point:
- 269.5±20.0 °C(Predicted)
- Density
- 1.426±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
N-Bromosuccinimide Price
- Product number
- B801455
- Product name
- 4-Bromo-2-chloro-1-isopropoxybenzene
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- Z0344
- Product name
- 4-Bromo-2-chloro-1-isopropoxybenzene
- Packaging
- 5g
- Price
- $251
- Updated
- 2021/12/16
- Product number
- B1232
- Product name
- 4-bromo-2-chloro-1-(propan-2-yloxy)benzene
- Packaging
- 1g
- Price
- $661
- Updated
- 2021/12/16
- Product number
- B1232
- Product name
- 4-bromo-2-chloro-1-(propan-2-yloxy)benzene
- Packaging
- 5g
- Price
- $1728
- Updated
- 2021/12/16
- Product number
- A118279
- Product name
- 4-Bromo-2-chloro-1-isopropoxybenzene
- Purity
- 98%
- Packaging
- 250mg
- Price
- $9
- Updated
- 2021/12/16
2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE Chemical Properties,Usage,Production
Synthesis
3964-56-5
75-26-3
201849-21-0
General procedure for the synthesis of 4-bromo-2-chloro-1-isopropoxybenzene from 4-bromo-2-chlorophenol and 2-bromopropane: K2CO3 (100 g) and 2-bromopropane (136 mL) were added in one go to a stirred N,N-dimethylformamide (DMF) (250 mL) solution of 4-bromo-2-chlorophenol (50 g) at room temperature, under nitrogen protection. The reaction mixture was stirred at 85°C for 16 hours. After completion of the reaction, it was cooled to room temperature, the reaction mixture was filtered and the solvent in the filtrate was removed by distillation under reduced pressure. The residue was dissolved in ether (300 mL) and the organic phase was washed with water (6 x 100 mL) and subsequently dried and concentrated with MgSO4 to give 4-bromo-2-chlorophenyl 1-methylethyl ether (D10) (56 g) as a yellow oil. δH (CDCl3, 400 MHz): 1.37 (6H, d), 4.52 (1H, m), 6.82 (1H , d), 7.29 (1H, m), 7.50 (1H, d).
References
[1] Patent: WO2010/148649, 2010, A1. Location in patent: Page/Page column 85
[2] Patent: WO2011/113309, 2011, A1. Location in patent: Page/Page column 24-25
[3] Patent: US2011/269738, 2011, A1. Location in patent: Page/Page column 33
[4] Patent: WO2011/134280, 2011, A1. Location in patent: Page/Page column 66; 67
[5] Patent: US2013/12491, 2013, A1. Location in patent: Paragraph 0159; 0160
2-(4'-BROMO-2'-CHLOROPHENOXY)PROPANE Preparation Products And Raw materials
Raw materials
Preparation Products
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