Tributylammonium pyrophosphate

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Tributylammonium pyrophosphate

Product Name: Tributylammonium pyrophosphate
CAS No.: 5975-18-8
Chemical Name: Tributylammonium pyrophosphate
Synonyms: Bis(tributylaMMoniuM) Pyrophosphate;TRIBUTYLAMMONIUM PYROPHOSPHATE;PYROPHOSPHATE, TRIBUTYLAMMONIUM;Tri-n-butylammonium pyrophosphate, 95%;Tributyl Ammonium Pyrophosphate (TBAP);Bis(tri-n-butylammonium) pyrophosphate;Tributylammonium pyrophosphate (50% wt in ACN);Diphosphoric Acid compd. with N,N-Dibutyl-1-butanamine (1:2)
CBNumber: CB8743916
Molecular Formula: C12H31NO7P2
Formula Weight: 363.33
MOL File: 5975-18-8.mol

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Tributylammonium pyrophosphate Property

Melting point:: 78 - 83°C
storage temp.: -20°C
solubility: DMSO (Slightly), Methanol (Slightly), Water (Slightly)
form: Solid
color: White to Off-White
Stability:: Hygroscopic
InChI: InChI=1S/C12H27N.H4O7P2/c1-4-7-10-13(11-8-5-2)12-9-6-3;1-8(2,3)7-9(4,5)6/h4-12H2,1-3H3;(H2,1,2,3)(H2,4,5,6)
InChIKey: WJFREWBMJPXLBS-UHFFFAOYSA-N
SMILES: N(CCCC)(CCCC)CCCC.O(P(O)(O)=O)P(O)(O)=O

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Safety

WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: P8533
Product name: Tributylammonium pyrophosphate
Packaging: 1g
Price: $109.2
Updated: 2024/03/01

Sigma-Aldrich

Product number: P8533
Product name: Tributylammonium pyrophosphate
Packaging: 5g
Price: $585
Updated: 2024/03/01

Sigma-Aldrich

Product number: P8533
Product name: Tributylammonium pyrophosphate
Packaging: 250mg
Price: $64.9
Updated: 2024/03/01

Usbiological

Product number: 291000
Product name: Tributylammonium pyrophosphate
Packaging: 250mg
Price: $368
Updated: 2021/12/16

TRC

Product number: B585505
Product name: Bis(tributylammonium)Pyrophosphate
Packaging: 2.5g
Price: $205
Updated: 2021/12/16

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Tributylammonium pyrophosphate Chemical Properties,Usage,Production

Description

Tributylammonium pyrophosphate is a phosphorylating reagent used in the synthesis of phosphorylated nucleosides, particularly nucleoside triphosphates used as building blocks for the synthesis of DNA, RNA and sugar nucleotides; as well as a source of cellular energy. Nucleoside triphosphates are typically synthesised by treating free nucleosides with phosphorus oxychloride, then adding tributylammonium pyrophosphate to the reaction intermediate, where the lipophilic tributylammonium salt enhances solubility in organic solvents. Additionally, tributylammonium pyrophosphate was used in the preparation of structurally complex dinucleotide-5’-triphosphates.

Uses

Bis(tributylammonium) Pyrophosphate is an phosphorylating reagent used in the synthesis of phosphorylated deoxynucleosides.
Reactant for:
Enzymic synthesis of 3′-deoxy-apio-nucleic acid duplexes
Synthesis of deoxynucleoside S-methylphosphonic acids
Preparation of fluorescent non-nucleotide ATP analog N-methylanthraniloylamideethyl triphosphate
Useful in triphosphate synthesis because of its low water content and high solubility in organic solvents.

Uses

Reactant for:

Enzymic synthesis of 3′-deoxy-apio-nucleic acid duplexes
Synthesis of deoxynucleoside S-methylphosphonic acids
Preparation of fluorescent non-nucleotide ATP analog N-methylanthraniloylamideethyl triphosphate

Preparation

A solution of tetrasodium pyrophosphate (3.5 g, 7.5 mmol) in water (50 mL) was eluted through a cation exchange resin (BIO-RAD AG 50 W-X8 Resin, 50–100 mesh, hydrogen form) at 4 °C. The eluent with pH of less than 3 (pH paper) was collected directly into a vigorously stirred flask containing tributylamine (2 mL, 8 mmol, 4 °C). The obtained tributylammonium pyrophosphate was dried through repeated rotary evaporation with dry MeOH and then dissolved in dry DMF (10 mL).

References

Santner et al (2012). The synthesis of 2′-methylseleno adenosine and guanosine 5′-triphosphates. Bioorganic and Medicinal Chemistry 20:2416.
Hollenstein (2012). Nucleoside Triphosphates — Building Blocks for the Modification of Nucleic Acids. Molecules 17:13569-13591.
bramova et al (2007). A facile and effective synthesis of dinucleotide 5′-triphosphates. Bioorganic and Medicinal Chemistry 15:6549-6555.

Tributylammonium pyrophosphate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Tributylammonium pyrophosphate manufacturers

Xiamen Yunfan Biotech Co.,Ltd.

Product: Tributylammonium pyrophosphate 5975-18-8
Price: US $0.00-0.00/g
Min. Order: 100g
Purity: 99%+
Supply Ability: 100 Kilogram/Month
Release date: 2024-05-14

Henan Fengda Chemical Co., Ltd

Product: Tributylammonium pyrophosphate 5975-18-8
Price: US $8.00-6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-22

Career Henan Chemical Co

Product: TRIBUTYLAMMONIUM PYROPHOSPHATE 5975-18-8
Price: US $8.00/KG
Min. Order: 1KG
Purity: ＞98% HPLC
Supply Ability: 20 tons
Release date: 2020-02-17

5975-18-8, Tributylammonium pyrophosphateRelated Search:

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TRIBUTYLAMMONIUM PYROPHOSPHATE

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PYROPHOSPHATE, TRIBUTYLAMMONIUM

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Tributyl Ammonium Pyrophosphate (TBAP)

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5975-18-8

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