2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE
- Product Name
- 2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE
- CAS No.
- 5471-55-6
- Chemical Name
- 2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE
- Synonyms
- 2-CYCLOHEXYLETHANAMINE HCL;2-CYCLOHEXYL-ETHYLAMINE HCL;2-cyclohexylethanamine chloride;Cyclohexaneethanamine Hydrochloride;cyclohexaneethylamine,hydrochloride;2-Cyclohexyl-ethylamin hydrochloride;2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE;Cyclohexaneethanamine, hydrochloride (1:1);2-CYCLOHEXYLETHYLAMINE HYDROCHLORIDE ---CRYSTALLINE---
- CBNumber
- CB8758545
- Molecular Formula
- C8H18ClN
- Formula Weight
- 163.69
- MOL File
- 5471-55-6.mol
2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE Property
- storage temp.
- Sealed in dry,Room Temperature
- form
- Crystalline Powder
- color
- White
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 2921309990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H412Harmful to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P330Rinse mouth.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- C992120
- Product name
- 2-CyclohexylethylamineHydrochloride
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- C992120
- Product name
- 2-CyclohexylethylamineHydrochloride
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- AK-25118
- Product name
- 2-Cyclohexylethylaminehydrochloride
- Purity
- 98+%
- Packaging
- 1g
- Price
- $63
- Updated
- 2021/12/16
- Product number
- AK-25118
- Product name
- 2-Cyclohexylethylaminehydrochloride
- Purity
- 98+%
- Packaging
- 5g
- Price
- $252
- Updated
- 2021/12/16
- Product number
- FC139905
- Product name
- 2-Cyclohexylethanamine hydrochloride
- Packaging
- 5G
- Price
- $257
- Updated
- 2021/12/16
2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
3399-73-3
5471-55-6
Under argon protection, 2-(cyclohex-1-en-1-yl)ethylamine (500 mg, 4.00 mmol) was dissolved in methanol (10 mL) and 10% Pd/C (50 mg) was added. The reaction system was placed at 50°C, switched to hydrogen atmosphere (balloon pressure), and the reaction was stirred at room temperature for 16 hours. The reaction progress was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was filtered through diatomaceous earth and washed with methanol (2 x 5 mL). The filtrate was concentrated under reduced pressure to give the crude product. The crude product was ground with a solvent mixture of dichloromethane and ethyl acetate (1:1, 2 mL), followed by the addition of an ether solution of 1N hydrochloric acid (4 mL) to give 2-cyclohexylethylamine hydrochloride (261, 250 mg, 38%) as a white solid.TLC conditions: 20% ethyl acetate/hexane (Rf 0.3); 1H-NMR (DMSO-d6, 500 MHz): δ 7.79 (broad single peak, 2H), 2.77 (triple peak, J = 7.5 Hz, 2H), 1.66-1.59 (multiple peak, 5H), 1.45-1.41 (multiple peak, 2H), 1.32-1.28 (multiple peak, 1H), 1.23-1.11 (multiple peak, 3H), 0.91-0.84 (multiple peak, 2H).
References
[1] Patent: WO2015/138895, 2015, A1. Location in patent: Paragraph 000219
[2] Patent: US2010/113512, 2010, A1
[3] Patent: US2010/222345, 2010, A1. Location in patent: Page/Page column 107
[4] Patent: US2011/124559, 2011, A1
[5] Patent: CN102516115, 2016, B. Location in patent: Paragraph 0267-0269
2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE manufacturers
- Product
- 2-CYCLOHEXYL-ETHYLAMINE HYDROCHLORIDE 5471-55-6
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg,5kg,50kg
- Release date
- 2020-01-18