(2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE
- Product Name
- (2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE
- CAS No.
- 175461-34-4
- Chemical Name
- (2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE
- Synonyms
- 2,6-Dichloropyridine-4-yl-dimethylamine;2,6-Dichloro-N,N-dimethylpyridin-4-amine;4-Pyridinamine, 2,6-dichloro-N,N-dimethyl-;(2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE
- CBNumber
- CB8785604
- Molecular Formula
- C7H8Cl2N2
- Formula Weight
- 191.06
- MOL File
- Mol file
(2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 2870AQ
- Product name
- 2,6-Dichloro-N,N-dimethylpyridin-4-amine
- Packaging
- 1g
- Price
- $383.6
- Updated
- 2021/12/16
- Product number
- HCH0351174
- Product name
- (2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $499.36
- Updated
- 2021/12/16
- Product number
- CM127782
- Product name
- 2,6-dichloro-N,N-dimethylpyridin-4-amine
- Purity
- 98%
- Packaging
- 5g
- Price
- $561
- Updated
- 2021/12/16
- Product number
- 175461344
- Product name
- 2,6-Dichloro-N,N-dimethylpyridin-4-amine
- Packaging
- 5g
- Price
- $624
- Updated
- 2021/12/16
- Product number
- A102683
- Product name
- 2,6-Dichloro-N,N-dimethylpyridin-4-amine
- Purity
- 98%
- Packaging
- 100mg
- Price
- $26
- Updated
- 2021/12/16
(2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE Chemical Properties,Usage,Production
Synthesis
16063-69-7
506-59-2
175461-34-4
To 2,4,6-trichloropyridine (10.0 g, 55.6 mmol) and dimethylamine hydrochloride (4.5 g, 55.6 mmol) in N,N-dimethylformamide (DMF, 80 mL) was added triethylamine (Et3N, 8.0 g, 55.6 mmol). The reaction mixture was placed in a sealed tube, heated to 80 °C and maintained for 8 hours. After completion of the reaction, the mixture was diluted with water and extracted with ethyl acetate (EtOAc). The organic layers were combined, washed with saturated brine, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford the target product 2,6-dichloro-N,N-dimethylpyridin-4-amine (12-TT, 4.0 g) as a white solid.1H-NMR (DMSO-d6, 400 MHz): δ=6.66 (s, 2H), 2.99 (s, 6H).
References
[1] Patent: WO2014/31784, 2014, A1. Location in patent: Paragraph 0705
(2,6-DICHLORO-PYRIDIN-4-YL)-DIMETHYL-AMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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