IFLAB-BB F2108-0155

Product Name: IFLAB-BB F2108-0155
CAS No.: 95470-42-1
Chemical Name: IFLAB-BB F2108-0155
Synonyms: IFLAB-BB F2108-0155;Ethyl 2-Bromo-4-methylimidazole-5-carboxylate;Ethyl 2-bromo-4-methyl-1H-imidazole-5-carboxylate;Ethyl 2-broMo-5-Methyl-4H-iMidazole-4-carboxylate;ethyl 2-broMo-5-Methyl-1H-iMidazole-4-carboxylate;2-Bromo-4-methyl-1H-imidazole-5-carboxylic acid ethyl ester;2-Bromo-5-methyl-4H-imidazole-4-carboxylic acid ethyl ester;2-BROMO-5-METHYL-1H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER;2-BROMO-5-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER;1H-Imidazole-5-carboxylic acid,2-bromo-4-methyl-,ethyl ester
CBNumber: CB8828095
Molecular Formula: C7H9BrN2O2
Formula Weight: 233.06
MOL File: 95470-42-1.mol

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IFLAB-BB F2108-0155 Property

Melting point:: 152-153 °C
Boiling point:: 347.4±34.0 °C(Predicted)
Density: 1.576±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 8.81±0.10(Predicted)
Appearance: Colorless to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 128216
Product name: Ethyl2-bromo-4-methyl-1H-imidazole-5-carboxylate
Purity: 97%
Packaging: 1g
Price: $672
Updated: 2021/12/16

Matrix Scientific

Product number: 131730
Product name: Ethyl2-bromo-5-methyl-1H-imidazole-4-carboxylate
Purity: 97%
Packaging: 5g
Price: $1008
Updated: 2021/12/16

Matrix Scientific

Product number: 131730
Product name: Ethyl2-bromo-5-methyl-1H-imidazole-4-carboxylate
Purity: 97%
Packaging: 25g
Price: $3024
Updated: 2021/12/16

Ambeed

Product number: A315640
Product name: Ethyl2-bromo-4-methyl-1H-imidazole-5-carboxylate
Purity: 97%
Packaging: 25g
Price: $1173
Updated: 2021/12/16

Alichem

Product number: 95470421
Product name: Ethyl2-bromo-4-methyl-1H-imidazole-5-carboxylate
Packaging: 10g
Price: $1333.78
Updated: 2021/12/16

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IFLAB-BB F2108-0155 Chemical Properties,Usage,Production

Synthesis

51605-32-4

95470-42-1

General procedure: The synthesis of ethyl 2-bromo-4-methyl-1H-imidazole-5-carboxylate (EV-AT8648-001) from ethyl 4-methyl-5-imidazolecarboxylate was performed as follows: Step 1: To a stirred solution of ethyl 4-methyl-1H-imidazole-5-carboxylate (CAS 51605-32-4, 500 mg, 3.24 mmol) in a mixture of acetonitrile (10 mL) and chloroform (10 mL), N-bromosuccinimide (577 mg, 3.24 mmol) was added. The reaction was carried out under nitrogen protection with stirring at room temperature for 18 hours. Upon completion of the reaction, the reaction mixture was concentrated and the residue was purified by fast column chromatography (eluent: 10-100% ethyl acetate/heptane gradient) to afford 560 mg (73% yield) of the target product, ethyl 2-bromo-4-methyl-1H-imidazole-5-carboxylate (EV-AT8648-001), as an off-white solid. LCMS analysis (Method D): retention time 0.87 min, mass spectrum m/z = 233/235 ([M+H]+).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 12, p. 3669 - 3674
[2] Patent: WO2017/147102, 2017, A1. Location in patent: Paragraph 00167-00168
[3] Patent: WO2008/111794, 2008, A1. Location in patent: Page/Page column 27
[4] Patent: US2009/156615, 2009, A1. Location in patent: Page/Page column 19
[5] Patent: US2015/284358, 2015, A1. Location in patent: Paragraph 0126; 0127; 0128

IFLAB-BB F2108-0155 Preparation Products And Raw materials

Raw materials

Preparation Products

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IFLAB-BB F2108-0155 Suppliers

Canada 1 China 44 India 2 United Kingdom 1 United States 9 Global 57

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95470-42-1, IFLAB-BB F2108-0155Related Search:

2-BROMO-3,5-DIMETHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER IFLAB-BB F2108-0155

IFLAB-BB F2108-0155

2-BROMO-5-METHYL-3H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER

2-BROMO-5-METHYL-1H-IMIDAZOLE-4-CARBOXYLIC ACID ETHYL ESTER

2-Bromo-5-methyl-4H-imidazole-4-carboxylic acid ethyl ester

ethyl 2-broMo-5-Methyl-1H-iMidazole-4-carboxylate

Ethyl 2-broMo-5-Methyl-4H-iMidazole-4-carboxylate

Ethyl 2-bromo-4-methyl-1H-imidazole-5-carboxylate

1H-Imidazole-5-carboxylic acid,2-bromo-4-methyl-,ethyl ester

1H-Imidazole-4-carboxylic acid, 2-bromo-5-methyl-, ethyl ester

Ethyl 2-Bromo-4-methylimidazole-5-carboxylate

2-Bromo-4-methyl-1H-imidazole-5-carboxylic acid ethyl ester

95470-42-1