ChemicalBook > CAS DataBase List > METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE

METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE

Product Name: METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
CAS No.: 4093-88-3
Chemical Name: METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
Synonyms: N-METHYL-3-NITROPYRIDIN-2-AMINE;2-(Methylamino)-3-nitropyridine;N-METHYL-3-NITRO-2-PYRIDINAMINE;methyl-(3-nitro-2-pyridyl)amine;2-Pyridinamine, N-methyl-3-nitro-;METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
CBNumber: CB8848400
Molecular Formula: C6H7N3O2
Formula Weight: 153.14
MOL File: 4093-88-3.mol

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METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Property

Melting point:: 67-69
Boiling point:: 262-262.5 °C(Press: 740 Torr)
Density: 1.343±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 2.87±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B426508
Product name: N-Methyl-3-nitropyridin-2-amine
Packaging: 50mg
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-Y8
Product name: 2-(Methylamino)-3-nitropyridine
Packaging: 250mg
Price: $35
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-Y8
Product name: 2-(Methylamino)-3-nitropyridine
Packaging: 1g
Price: $105
Updated: 2021/12/16

AK Scientific

Product number: V5831
Product name: N-Methyl-3-nitropyridin-2-amine
Packaging: 5g
Price: $271
Updated: 2021/12/16

Matrix Scientific

Product number: 032311
Product name: N-Methyl-3-nitro-2-pyridinamine
Packaging: 500mg
Price: $342
Updated: 2021/12/16

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METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Chemical Properties,Usage,Production

Synthesis

5470-18-8

4093-88-3

Synthesis of N-methyl-3-nitropyridin-2-amine: methylamine (33% ethanol solution, 110 mL, 883 mmol) was added to a 500 mL three-necked round-bottomed flask and cooled to 0 °C in an ice bath. Under stirring, 2-chloro-3-nitropyridine (20 g, 126 mmol) was added in batches, and care was taken to control the dosing rate to alleviate the exothermic reaction. After the addition was completed, the reaction mixture was continued to be stirred at 0 °C for 2 h, followed by slow warming to room temperature and stirring for 1 h. The reaction was then concentrated under reduced pressure. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure and the residue was dissolved in 500 mL of water and extracted with ethyl acetate (3 x 150 mL). The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the bright orange-yellow solid product N-methyl-3-nitropyridin-2-amine (19 g, 98.5% yield).

References

[1] Patent: US2012/228583, 2012, A1

METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE 4093-88-3
Price: US $30.00-20.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2024-08-01

4093-88-3, METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINERelated Search:

2-METHYLAMINO-3-NITRO-5-(TRIFLUOROMETHYL)PYRIDINE N2-CYCLOPROPYL-3-NITROPYRIDIN-2-AMINE 1-METHYL-1-(3-NITRO-2-PYRIDYL)HYDRAZINE 1-(3-NITROPYRIDIN-2-YL)PIPERIDINE-4-CARBONITRILE 1-(3-NITROPYRIDIN-2-YL)PIPERIDINE-4-CARBOXAMIDE DNPYR-DL-NORLEUCINE DNPYR-L-ISOLEUCINE MONOCYCLOHEXYL AMMONI UM METHYL-(4-METHYL-3-NITRO-PYRIDIN-2-YL)-AMINE METHYL-(6-METHYL-3-NITRO-PYRIDIN-2-YL)-AMINE DNPY-DL-ALANINE N-[3-(1H-imidazol-1-yl)propyl]-3-nitropyridin-2-amine N-(4-CHLOROBENZYL)-3-NITRO-2-PYRIDINAMINE 3-nitro-N-(pyridin-3-ylmethyl)pyridin-2-amine DNPY-GLYCINE N1-(1-BROMO-4-NITRO-3-ISOQUINOLYL)BENZAMIDE N'1-METHYL-N'1-(3-NITRO-2-PYRIDYL)-2,3,3-TRICHLOROPROP-2-ENOHYDRAZIDE 3-(2-[1-(3-NITRO-2-PYRIDINYL)-4-PIPERIDINYLIDENE]HYDRAZINO)-2(1H)-QUINOXALINONE 3-nitro-N-(pyridin-2-ylmethyl)pyridin-2-amine

N-METHYL-3-NITRO-2-PYRIDINAMINE

2-(Methylamino)-3-nitropyridine

N-METHYL-3-NITROPYRIDIN-2-AMINE

METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE

2-Pyridinamine, N-methyl-3-nitro-

methyl-(3-nitro-2-pyridyl)amine

4093-88-3