indan-1-carbonitrile
- Product Name
- indan-1-carbonitrile
- CAS No.
- 26452-97-1
- Chemical Name
- indan-1-carbonitrile
- Synonyms
- indan-1-carbonitrile;2,3-dihydro-1H-indene-1-carbonitrile;1H-Indene-1-carbonitrile, 2,3-dihydro-;2,3-dihydro-1H-indene-1-carbonitrile - [AC80475]
- CBNumber
- CB8896027
- Molecular Formula
- C10H9N
- Formula Weight
- 143.19
- MOL File
- 26452-97-1.mol
indan-1-carbonitrile Property
- Boiling point:
- 108-109 °C(Press: 0.7 Torr)
- Density
- 1.09±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D679825
- Product name
- 2,3-Dihydro-1H-indene-1-carbonitrile
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FD142040
- Product name
- 2,3-Dihydro-1H-indene-1-carbonitrile
- Packaging
- 100mg
- Price
- $70
- Updated
- 2021/12/16
- Product number
- FD142040
- Product name
- 2,3-Dihydro-1H-indene-1-carbonitrile
- Packaging
- 250mg
- Price
- $140
- Updated
- 2021/12/16
- Product number
- FD142040
- Product name
- 2,3-Dihydro-1H-indene-1-carbonitrile
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- FD142040
- Product name
- 2,3-Dihydro-1H-indene-1-carbonitrile
- Packaging
- 1g
- Price
- $418.75
- Updated
- 2021/12/16
indan-1-carbonitrile Chemical Properties,Usage,Production
Synthesis
29872-81-9
26452-97-1
The general procedure for the synthesis of 2,3-dihydro-1H-indene-1-carbonitrile from 1H-indene-3-carbonitrile (CAS:29872-81-9) was as follows: 5% Pd/C catalyst was suspended in ethanol (200 mL) solution of 1H-indene-3-carbonitrile, and the reaction was carried out with vigorous stirring under hydrogen atmosphere overnight. Upon completion of the reaction, the excess hydrogen was removed, followed by filtration of the reaction mixture through a diatomaceous earth pad and concentration of the filtrate to obtain an oily material. This oily substance was redissolved in ethanol and a second filtration was performed to completely remove residual catalyst and carbon. Finally, the solvent was removed by evaporation to give 12.0108 g of 2,3-dihydro-1H-indene-1-carbonitrile in 95% yield and the product as an oil. The structure of the product was confirmed by 1H NMR (400 MHz, DMSO-D6): δ 2.2 (m, 1H), 2.5 (m, 1H), 2.9 (m, 1H), 3.0 (m, 1H), 4.4 (t, J = 8.0 Hz, 1H), 7.2 (m, 2H), 7.3 (m, 1H), 7.4 (m, J = 7.7, 4.9 Hz, 1H).
References
[1] Patent: WO2004/55012, 2004, A1. Location in patent: Page 53
indan-1-carbonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from indan-1-carbonitrile manufacturers
- Product
- indan-1-carbonitrile 26452-97-1
- Price
- US $5.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12