2-Fluoro-4-Iodophenol
- Product Name
- 2-Fluoro-4-Iodophenol
- CAS No.
- 2713-28-2
- Chemical Name
- 2-Fluoro-4-Iodophenol
- Synonyms
- 2-Fluoro-4-Iodopheno;O-Fluoro-P-Iodophenol;2-Fluoro-4-Iodophenol;4-Iodo-2-fluorophenol;4-iodine-2-fluorophenol;Phenol,2-fluoro-4-iodo-
- CBNumber
- CB8948858
- Molecular Formula
- C6H4FIO
- Formula Weight
- 238
- MOL File
- Mol file
2-Fluoro-4-Iodophenol Property
- Boiling point:
- 238.1±25.0 °C(Predicted)
- Density
- 2.085±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Store in freezer, under -20°C
- pka
- 8.10±0.18(Predicted)
- form
- solid
- color
- Light yellow to yellow
Safety
- HS Code
- 2908190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
N-Bromosuccinimide Price
- Product number
- CS-W005152
- Product name
- 2-Fluoro-4-iodophenol
- Purity
- 99.94%
- Packaging
- 5g
- Price
- $121
- Updated
- 2021/12/16
- Product number
- PC56141
- Product name
- 2-Fluoro-4-iodophenol
- Packaging
- 1g
- Price
- $174
- Updated
- 2021/12/16
- Product number
- HCH0063128
- Product name
- 2-FLUORO-4-IODOPHENOL
- Purity
- 95.00%
- Packaging
- 100MG
- Price
- $174.3
- Updated
- 2021/12/16
- Product number
- 096029
- Product name
- 2-Fluoro-4-iodophenol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $189
- Updated
- 2021/12/16
- Product number
- CS-W005152
- Product name
- 2-Fluoro-4-iodophenol
- Purity
- 99.94%
- Packaging
- 10g
- Price
- $202
- Updated
- 2021/12/16
2-Fluoro-4-Iodophenol Chemical Properties,Usage,Production
Synthesis
367-12-4
2713-28-2
General procedure for the synthesis of 2-fluoro-4-iodophenol from 2-fluorophenol: Iodine (1.06 g, 4.18 mmol) was added in a single addition to a stirring solution of 2-fluorophenol (0.47 g, 4.18 mmol) in concentrated ammonia (22 ml) at room temperature. The reaction mixture was stirred overnight at room temperature and the solvent was removed by evaporation under reduced pressure. The residue was partitioned between ethyl acetate (100 ml) and water (40 ml). The organic phase was washed sequentially with 5% sodium bisulfite solution and brine (10 ml), dried over anhydrous magnesium sulfate and filtered, and the filtrate was concentrated to dryness under reduced pressure. The residue was purified by silica gel column chromatography (dichloromethane/ethyl acetate, 9:1) to afford 2-fluoro-4-iodophenol (0.42 g, 42% yield) as a colorless solid.1H-NMR (CDCl3) δ 7.3-7.4 (m, 2H), 6.75 (t, J=8.8 Hz, 1H), 5.17 (s, 1H).
References
[1] Tetrahedron Letters, 2010, vol. 51, # 16, p. 2170 - 2173
[2] Patent: WO2014/63199, 2014, A1. Location in patent: Page/Page column 94
[3] Canadian Journal of Chemistry, 1965, vol. 43, p. 650 - 658
[4] Patent: EP409634, 1991, A2
[5] Patent: EP409634, 1991, A2
2-Fluoro-4-Iodophenol Preparation Products And Raw materials
Raw materials
Preparation Products
2-Fluoro-4-Iodophenol Suppliers
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View Lastest Price from 2-Fluoro-4-Iodophenol manufacturers
- Product
- 2-Fluoro-4-Iodophenol 2713-28-2
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 200KG
- Release date
- 2020-01-07