3-NITRO-4-METHYLOPHENYLACETIC ACID

Product Name: 3-NITRO-4-METHYLOPHENYLACETIC ACID
CAS No.: 54941-44-5
Chemical Name: 3-NITRO-4-METHYLOPHENYLACETIC ACID
Synonyms: 4-Methyl-3-nitrophenylacetic acid;3-NITRO-4-METHYLOPHENYLACETIC ACID;Benzeneacetic acid, 4-methyl-3-nitro-;4-(Carboxymethyl)-3-nitrotoluene, 5-(Carboxymethyl)-2-methylnitrobenzene;4-(Carboxymethyl)-2-nitrotoluene, 5-(Carboxymethyl)-2-methylnitrobenzene
CBNumber: CB91010399
Molecular Formula: C9H9NO4
Formula Weight: 195.17
MOL File: 54941-44-5.mol

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3-NITRO-4-METHYLOPHENYLACETIC ACID Property

Boiling point:: 374.5±27.0 °C(Predicted)
Density: 1.346±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.14±0.10(Predicted)
form: solid
color: Yellow

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M339578
Product name: 2-(4-Methyl-3-nitrophenyl)aceticAcid
Packaging: 500mg
Price: $110
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-Z7
Product name: 4-Methyl-3-nitrophenylacetic acid
Packaging: 250mg
Price: $152
Updated: 2021/12/16

AK Scientific

Product number: J96578
Product name: 2-(4-Methyl-3-nitrophenyl)aceticacid
Packaging: 1g
Price: $79
Updated: 2021/12/16

AK Scientific

Product number: J96578
Product name: 2-(4-Methyl-3-nitrophenyl)aceticacid
Packaging: 5g
Price: $238
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-Z7
Product name: 4-Methyl-3-nitrophenylacetic acid
Packaging: 1g
Price: $312
Updated: 2021/12/16

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3-NITRO-4-METHYLOPHENYLACETIC ACID Chemical Properties,Usage,Production

Synthesis

622-47-9

54941-44-5

A. Synthesis of 3-nitro-4-methylphenylacetic acid To a dry dichloromethane solution of 4-methylphenylacetic acid (1.50 g, 10.0 mmol) was added dropwise fuming nitric acid (1.5 mL). The reaction mixture was stirred at room temperature for 2 h. The reaction was subsequently quenched with water. The reaction mixture was extracted with ethyl acetate and the organic phase was washed sequentially twice with water and once with brine. The organic layer was dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to give 3-nitro-4-methylphenylacetic acid (1.66 g, 85% yield). The product was characterized as follows: 1H NMR (CDCl3) δ 7.91 (d, 1H), 7.42 (dd, 1H), 7.31 (d, 1H), 3.71 (s, 2H), 2.58 (s, 3H); ES-MS m/z 196 [M + H]+.

References

[1] Patent: US6593322, 2003, B1
[2] Patent: WO2003/90912, 2003, A1. Location in patent: Page/Page column 117
[3] Journal fuer Praktische Chemie (Leipzig), 1891, vol. <2> 44, p. 85
[4] Patent: WO2014/145022, 2014, A1. Location in patent: Page/Page column 52

3-NITRO-4-METHYLOPHENYLACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3-NITRO-4-METHYLOPHENYLACETIC ACID Suppliers

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View Lastest Price from 3-NITRO-4-METHYLOPHENYLACETIC ACID manufacturers

Career Henan Chemical Co

Product: 3-NITRO-4-METHYLOPHENYLACETIC ACID 54941-44-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-09

54941-44-5, 3-NITRO-4-METHYLOPHENYLACETIC ACIDRelated Search:

(2S)-2-AMINO-2-[4-(TERT-BUTYL)-2,6-DIMETHYL-3,5-DINITROPHENYL]PROPANOIC ACID 3-NITRO-4-METHYLOPHENYLACETIC ACID AMINO-(3-NITRO-4-TRIFLUOROMETHYL-PHENYL)-ACETIC ACID (2S)-2-AMINO-2-(4-METHYL-3-NITROPHENYL)PROPANOIC ACID (2R)-2-AMINO-2-[4-(TERT-BUTYL)-2,6-DIMETHYL-3,5-DINITROPHENYL]PROPANOIC ACID AMINO-(4-METHYL-3-NITRO-PHENYL)-ACETIC ACID (2R)-2-AMINO-2-(4-METHYL-3-NITROPHENYL)PROPANOIC ACID

3-NITRO-4-METHYLOPHENYLACETIC ACID

4-(Carboxymethyl)-2-nitrotoluene, 5-(Carboxymethyl)-2-methylnitrobenzene

4-Methyl-3-nitrophenylacetic acid

4-(Carboxymethyl)-3-nitrotoluene, 5-(Carboxymethyl)-2-methylnitrobenzene

Benzeneacetic acid, 4-methyl-3-nitro-

54941-44-5