ChemicalBook > CAS DataBase List > Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI)

Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI)

Product Name: Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.: 167216-30-0
Chemical Name: Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI)
Synonyms: 4-(Boc-amino)-2-butanol;tert-Butyl (3-hydroxybutyl);tert-Butyl (3-hydroxybutyl)carbaMate;tert-butyl N-(3-hydroxybutyl)carbamate;N-(3-hydroxybutyl)carbamic acid tert-butyl ester;(3-Hydroxybutyl)-carbamic acid 1,1-dimethylethyl ester;CarbaMic acid, (3-hydroxybutyl)-, 1,1-diMethylethyl ester;Carbamic acid, N-(3-hydroxybutyl)-, 1,1-dimethylethyl ester;Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI)
CBNumber: CB91058498
Molecular Formula: C9H19NO3
Formula Weight: 189.25
MOL File: 167216-30-0.mol

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Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI) Property

Boiling point:: 301.4±25.0 °C(Predicted)
Density: 1.010±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 12.75±0.46(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB130818
Product name: tert-Butyl (3-hydroxybutyl)carbamate
Packaging: 250mg
Price: $57.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130818
Product name: tert-Butyl (3-hydroxybutyl)carbamate
Packaging: 500mg
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130818
Product name: tert-Butyl (3-hydroxybutyl)carbamate
Packaging: 1g
Price: $170
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130818
Product name: tert-Butyl (3-hydroxybutyl)carbamate
Packaging: 2g
Price: $289
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130818
Product name: tert-Butyl (3-hydroxybutyl)carbamate
Packaging: 5G
Price: $578
Updated: 2021/12/16

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Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI) Chemical Properties,Usage,Production

Synthesis

24424-99-5

114963-62-1

167216-30-0

Step 1: Synthesis of tert-butyl (3-hydroxybutyl)carbamate To a stirred solution of (R)-4-aminobutan-2-ol (1.0 g, 11.2 mmol) in dichloromethane (20 mL) was slowly added a solution of di-tert-butyl dicarbonate (2.45 g, 11.2 mmol) in dichloromethane (20 mL). The reaction mixture was stirred at room temperature for 18 hours. After completion of the reaction, the organic phase was washed sequentially with aqueous citric acid and saturated aqueous sodium bicarbonate, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to afford the title compound tert-butyl (3-hydroxybutyl)carbamate as a colorless oil (2.1 g, 99% yield).

References

[1] Patent: WO2011/71725, 2011, A1. Location in patent: Page/Page column 55
[2] Patent: WO2011/71716, 2011, A1. Location in patent: Page/Page column 55
[3] Russian Journal of Bioorganic Chemistry, 2011, vol. 37, # 2, p. 225 - 230
[4] Patent: US5610195, 1997, A

Carbamic acid, (3-hydroxybutyl)-, 1,1-dimethylethyl ester (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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