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Piperazine, 1,4-diacetyl- (6CI,8CI,9CI)

Product Name
Piperazine, 1,4-diacetyl- (6CI,8CI,9CI)
CAS No.
18940-57-3
Chemical Name
Piperazine, 1,4-diacetyl- (6CI,8CI,9CI)
Synonyms
1,4-DIACETYLPIPERAZINE;Piperazine, 1,4-diacetyl;1-(4-acetylpiperazin-1-yl)ethanone;1,1'-(1,4-Piperazinediyl)bisethanone;1,1'-(Piperazine-1,4-diyl)diethanone;1,1'-(Piperazine-1,4-diyl)bisethanone;Ethanone, 1,1'-(1,4-piperazinediyl)bis-;Piperazine, 1,4-diacetyl- (6CI,8CI,9CI);1,1'-(piperazine-1,4-diyl)bis(ethan-1-one)
CBNumber
CB91061083
Molecular Formula
C8H14N2O2
Formula Weight
170.21
MOL File
18940-57-3.mol
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Piperazine, 1,4-diacetyl- (6CI,8CI,9CI) Property

Boiling point:
365.2±35.0 °C(Predicted)
Density 
1.126±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
0.35±0.70(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
P992080
Product name
1,1''-(Piperazine-1,4-diyl)diethanone
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
P992080
Product name
1,1''-(Piperazine-1,4-diyl)diethanone
Packaging
500mg
Price
$155
Updated
2021/12/16
AK Scientific
Product number
9872AA
Product name
1,1'-(Piperazine-1,4-diyl)diethanone
Packaging
5g
Price
$489
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0976862
Product name
1,4-DIACETYL-PIPERAZINE
Purity
95.00%
Packaging
5MG
Price
$505.66
Updated
2021/12/16
Chemenu
Product number
CM147912
Product name
1,1''-(Piperazine-1,4-diyl)diethanone
Purity
95%
Packaging
5g
Price
$300
Updated
2021/12/16
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Piperazine, 1,4-diacetyl- (6CI,8CI,9CI) Chemical Properties,Usage,Production

Synthesis

110-85-0

108-24-7

18940-57-3

Piperazine (1 mmol) and acetic anhydride (2 mmol) were added to a 25 mL round-bottomed flask equipped with a magnetic stirrer, and SiO2/PDA-SO3H (30 mg, 1 mol/mL H+) was used as a catalyst. The reaction mixture was stirred at room temperature and the progress of the reaction was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was diluted with ethyl acetate and the catalyst was separated by centrifugation. Subsequently, the reaction mixture was washed with saturated NaHCO3 solution (1 x 15 mL) and the product was extracted with ethyl acetate (3 x 10 mL), dried over Na2SO4 and the solvent was evaporated under vacuum. The resulting product 1,1'-(piperazine-1,4-diyl)diethyl ketone is a compound known from literature.

References

[1] Catalysis Letters, 2018, vol. 148, # 9, p. 2734 - 2745
[2] Tetrahedron Letters, 2002, vol. 43, # 23, p. 4261 - 4265
[3] Chemische Berichte, 1897, vol. 30, p. 1585
[4] Farmaco, 1992, vol. 47, # 5, p. 599 - 605

Piperazine, 1,4-diacetyl- (6CI,8CI,9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Piperazine, 1,4-diacetyl- (6CI,8CI,9CI) Suppliers

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View Lastest Price from Piperazine, 1,4-diacetyl- (6CI,8CI,9CI) manufacturers

Honest Joy Holdings Limited
Product
1-(4-acetylpiperazin-1-yl)ethanone 18940-57-3
Price
US $0.00/KG
Min. Order
1KG
Purity
98.9%
Supply Ability
100 tons
Release date
2022-01-14