Pyridine, 2-bromo-5-(chloromethyl)- (9CI)

Product Name: Pyridine, 2-bromo-5-(chloromethyl)- (9CI)
CAS No.: 168173-56-6
Chemical Name: Pyridine, 2-bromo-5-(chloromethyl)- (9CI)
Synonyms: 2-Fluoro-11-(methylthio)pyridine;2-BroMo-5-(chloroMethyl)pyridine;Pyridine, 2-bromo-5-(chloromethyl)-;Pyridine, 2-bromo-5-(chloromethyl)- (9CI);7-(diethylamino)-3-(1,3-dimethylbenzimidazol-3-ium-2-yl)chromen-2-one,
CBNumber: CB91067979
Molecular Formula: C6H5BrClN
Formula Weight: 206.47
MOL File: 168173-56-6.mol

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Pyridine, 2-bromo-5-(chloromethyl)- (9CI) Property

Boiling point:: 285.0±25.0 °C(Predicted)
Density: 1.631±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 0.02±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 8204CP
Product name: 2-Bromo-5-(chloromethyl)pyridine
Packaging: 250mg
Price: $178
Updated: 2021/12/16

AK Scientific

Product number: 8204CP
Product name: 2-Bromo-5-(chloromethyl)pyridine
Packaging: 10g
Price: $2468
Updated: 2021/12/16

Labseeker

Product number: SC-35198
Product name: 2-BROMO-5-(CHLOROMETHYL)PYRIDINE
Purity: 95
Packaging: 5g
Price: $2658
Updated: 2021/12/16

Ambeed

Product number: A295347
Product name: 2-Bromo-5-(chloromethyl)pyridine
Purity: 95%
Packaging: 100mg
Price: $122
Updated: 2021/12/16

Ambeed

Product number: A295347
Product name: 2-Bromo-5-(chloromethyl)pyridine
Purity: 95%
Packaging: 250mg
Price: $182
Updated: 2021/12/16

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Pyridine, 2-bromo-5-(chloromethyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

122306-01-8

168173-56-6

General procedure for the synthesis of 2-bromo-5-(chloromethyl)pyridine from 2-bromo-5-(hydroxymethyl)pyridine: (6-bromopyridin-3-yl)methanol (1.000 g) was dissolved in dichloromethane (DCM, 10 mL) and cooled to 0°C. Thionyl chloride (1.260 g) was added slowly dropwise with stirring. After the dropwise addition was completed, the ice bath was removed and the reaction mixture was allowed to warm naturally to room temperature and stirring was continued for 2 hours. Upon completion of the reaction, the reaction solution was concentrated directly to give 1.050 g of 2-bromo-5-(chloromethyl)pyridine.

References

[1] Patent: WO2006/114213, 2006, A1. Location in patent: Page/Page column 30
[2] Patent: US5420270, 1995, A
[3] Journal of Medicinal Chemistry, 2012, vol. 55, # 7, p. 3201 - 3215
[4] Inorganic Chemistry, 2016, vol. 55, # 16, p. 7944 - 7953
[5] Journal of Biological Inorganic Chemistry, 2018, vol. 23, # 7, p. 1139 - 1151

Pyridine, 2-bromo-5-(chloromethyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Pyridine, 2-bromo-5-(chloromethyl)- (9CI) Suppliers

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168173-56-6, Pyridine, 2-bromo-5-(chloromethyl)- (9CI)Related Search:

Pyridine, 2-bromo-5-(chloromethyl)- (9CI)

2-BroMo-5-(chloroMethyl)pyridine

Pyridine, 2-bromo-5-(chloromethyl)-

7-(diethylamino)-3-(1,3-dimethylbenzimidazol-3-ium-2-yl)chromen-2-one,

2-Fluoro-11-(methylthio)pyridine

168173-56-6

PYRIDINE