6-methoxy-2-phenyl-tetralone
- Product Name
- 6-methoxy-2-phenyl-tetralone
- CAS No.
- 1769-84-2
- Chemical Name
- 6-methoxy-2-phenyl-tetralone
- Synonyms
- 6-Methoxy-2-phenyltetralone;6-Methoxy-2-phenyl-1-tetralone;6-Methoxy-2-phenylnaphthalen-1(4H)-one;6-Methoxy-2-phenyl-3,4-dihydronaphthalen-1(2H);6-Methoxy-2-phenyl-3,4-dihydronaphthalen-1(2H)-one;3,4-dihydro-6-methoxy-2-phenyl-1(2H)-Naphthalenone;6-methoxy-2-phenyl-3,4-dihydro-2H-naphthalen-1-one;1(2H)-Naphthalenone, 3,4-dihydro-6-methoxy-2-phenyl-;6-methoxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-one
- CBNumber
- CB91117973
- Molecular Formula
- C17H16O2
- Formula Weight
- 252.31
- MOL File
- 1769-84-2.mol
6-methoxy-2-phenyl-tetralone Property
- Melting point:
- 113-116 °C
- Boiling point:
- 429.9±45.0 °C(Predicted)
- Density
- 1.141±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder
- color
- Yellow
Safety
- HS Code
- 2914500090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- Y1137
- Product name
- 6-Methoxy-2-phenyl-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 1g
- Price
- $251
- Updated
- 2021/12/16
- Product number
- OR943451
- Product name
- 6-Methoxy-2-phenyl-tetralone
- Packaging
- 1g
- Price
- $254
- Updated
- 2021/12/16
- Product number
- 2617-1-0A
- Product name
- 6-Methoxy-2-phenyltetralone
- Packaging
- 1g
- Price
- $280
- Updated
- 2021/12/16
- Product number
- OR943451
- Product name
- 6-Methoxy-2-phenyl-tetralone
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 2617-1-0A
- Product name
- 6-Methoxy-2-phenyltetralone
- Packaging
- 250mg
- Price
- $144
- Updated
- 2021/12/16
6-methoxy-2-phenyl-tetralone Chemical Properties,Usage,Production
Synthesis
108-90-7
1078-19-9
1769-84-2
A Schlenk flask was charged with 6-methoxy-3,4-dihydronaphthalen-1(2H)-one (1,352 mg, 2.0 mmol), sodium tert-butanolate (365 mg, 3.8 mmol) and Pd-132 (1.4 mg, 0.002 mmol). The flask was sealed with a rubber stopper, evacuated three times and backfilled with nitrogen operation. Chlorobenzene (0.20 mL, 2.0 mmol) was added to the flask via a gas-tight syringe, followed by dioxane (2.0 mL). The reaction mixture was stirred at 100°C for 18 hours. After completion of the reaction, the mixture was filtered through a silica gel column and the silica gel pad was washed with methyl tert-butyl ether (MTBE, 20 mL). The filtrate was concentrated to give the off-white solid product 6-methoxy-2-phenyltetralone (455 mg, 90% yield). The structure of the product was confirmed by 1H NMR (CDCl3) and 13C NMR (CDCl3).
References
[1] Chemistry - A European Journal, 2014, vol. 20, # 52, p. 17272 - 17276
[2] Patent: WO2012/159981, 2012, A2. Location in patent: Page/Page column 20
[3] Organic and Biomolecular Chemistry, 2015, vol. 13, # 34, p. 9012 - 9021
6-methoxy-2-phenyl-tetralone Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-methoxy-2-phenyl-tetralone manufacturers
- Product
- 6-methoxy-2-phenyl-tetralone 1769-84-2
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2019-12-26