6-CHLORO-3-NITROQUINOLIN-4-OL
- Product Name
- 6-CHLORO-3-NITROQUINOLIN-4-OL
- CAS No.
- 101861-61-4
- Chemical Name
- 6-CHLORO-3-NITROQUINOLIN-4-OL
- Synonyms
- 6-chloro-3-nitro-4-Quinolinol;4-Quinolinol,6-chloro-3-nitro-;6-CHLORO-3-NITROQUINOLIN-4-OL;6-chloro-3-nitro-1H-quinolin-4-one;6-Chloro-3-nitroquinolin-4-ol, CAS 101861-61-4
- CBNumber
- CB91119250
- Molecular Formula
- C9H5ClN2O3
- Formula Weight
- 224.6
- MOL File
- 101861-61-4.mol
6-CHLORO-3-NITROQUINOLIN-4-OL Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 8121DC
- Product name
- 6-Chloro-3-nitroquinolin-4-ol
- Packaging
- 5g
- Price
- $277
- Updated
- 2021/12/16
- Product number
- HCH0025180
- Product name
- 6-CHLORO-3-NITROQUINOLIN-4-OL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $727.65
- Updated
- 2021/12/16
- Product number
- A149721
- Product name
- 6-Chloro-3-nitroquinolin-4-ol
- Purity
- 98%
- Packaging
- 25g
- Price
- $883
- Updated
- 2021/12/16
- Product number
- 101861614
- Product name
- 6-Chloro-3-nitroquinolin-4-ol
- Packaging
- 100g
- Price
- $1595.8
- Updated
- 2021/12/16
- Product number
- CM145216
- Product name
- 6-chloro-3-nitroquinolin-4-ol
- Purity
- 98%
- Packaging
- 10g
- Price
- $295
- Updated
- 2021/12/16
6-CHLORO-3-NITROQUINOLIN-4-OL Chemical Properties,Usage,Production
Synthesis
102014-85-7
101861-61-4
Step 2: Synthesis of 6-chloro-3-nitroquinolin-4-ol To a 500 mL round bottom flask was added 5-chloro-2-(2-nitroethylideneamino)benzoic acid (25 g, 0.10 mol), K2CO3 (42.6 g, 0.30 mol) and acetic anhydride (250 mL). The reaction mixture was heated to 90 °C and the reaction was stirred at this temperature for 1 hour. Upon completion of the reaction, the resulting solid product was collected by filtration, washed sufficiently with deionized water to remove residual reactants and salts, and subsequently dried to afford 17.5 g (76% yield) of 6-chloro-3-nitroquinolin-4-ol as a gray solid. The structure of the product was confirmed by 1H NMR (300 MHz, DMSO-d6): δ 9.12 (s, 1H), 8.15 (s, 1H), 7.72 (s, 2H). Mass spectral analysis showed m/z: 224 (M+H+).
References
[1] Patent: US2010/120741, 2010, A1. Location in patent: Page/Page column 93
[2] Patent: WO2011/112731, 2011, A2. Location in patent: Page/Page column 199-200
6-CHLORO-3-NITROQUINOLIN-4-OL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-CHLORO-3-NITROQUINOLIN-4-OL manufacturers
- Product
- 6-CHLORO-3-NITROQUINOLIN-4-OL 101861-61-4
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-10