2-AMINO-4-IODOBENZOIC ACID
- Product Name
- 2-AMINO-4-IODOBENZOIC ACID
- CAS No.
- 20776-54-9
- Chemical Name
- 2-AMINO-4-IODOBENZOIC ACID
- Synonyms
- 2-AMINO-4-IODOBENZOIC ACID;Benzoic acid, 2-amino-4-iodo-
- CBNumber
- CB91119553
- Molecular Formula
- C7H6INO2
- Formula Weight
- 263.03
- MOL File
- 20776-54-9.mol
2-AMINO-4-IODOBENZOIC ACID Property
- Melting point:
- 208 °C (decomp)(Solv: ethanol (64-17-5))
- Boiling point:
- 377.0±37.0 °C(Predicted)
- Density
- 2.082±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 4.76±0.10(Predicted)
- Appearance
- Off-white to light brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A630478
- Product name
- 2-Amino-4-iodobenzoicAcid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- A630478
- Product name
- 2-Amino-4-iodobenzoicAcid
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- AK-34047
- Product name
- 2-Amino-4-iodobenzoicacid
- Purity
- 97%
- Packaging
- 1g
- Price
- $51
- Updated
- 2021/12/16
- Product number
- FA142361
- Product name
- 2-Amino-4-iodobenzoic acid
- Packaging
- 1g
- Price
- $69
- Updated
- 2021/12/16
- Product number
- W4360
- Product name
- 2-Amino-4-iodobenzoicacid
- Packaging
- 250mg
- Price
- $86
- Updated
- 2021/12/16
2-AMINO-4-IODOBENZOIC ACID Chemical Properties,Usage,Production
Synthesis
116529-62-5
20776-54-9
B. Synthesis of 2-amino-4-iodobenzoic acid: 4-Iodo-2-nitrobenzoic acid (20 g, 68 mmol, 1.0 eq.) was dissolved in 200 mL of ethyl acetate, followed by addition of stannous chloride dihydrate (SnCl2-2H2O, 46 g, 204 mmol, 3.0 eq.) in three batches. The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the pH of the mixture was adjusted slowly by adding saturated aqueous sodium bicarbonate solution to 9. The precipitated solids were removed by filtration through diatomaceous earth and washed with distilled water. The aqueous layer in the filtrate was separated and acidified with concentrated hydrochloric acid to pH=2. The precipitated solid was collected by filtration and dried to give 2-amino-4-iodobenzoic acid as a white solid (19 g, 68 mmol, 100% yield).1H NMR (400 MHz, CD3OD) and 1H NMR (500 MHz, CDCl3) data were as follows: δ 7.56 (d, J=8.5 Hz, 1H), 7.08 (s, 1H), 6.99 (d, J=8.5 Hz, 1H), 5.71 (br s, 2H).
References
[1] Patent: US2006/69286, 2006, A1. Location in patent: Page/Page column 26
[2] American Chemical Journal, 1910, vol. 44, p. 448
2-AMINO-4-IODOBENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
2-AMINO-4-IODOBENZOIC ACID Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 0535-6385396
- Fax
- +86 (535) 638-9971
- info@carbottpharm.com
- Country
- China
- ProdList
- 957
- Advantage
- 56
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- +86 21 61551611
- Fax
- +86 21 50676805
- Country
- China
- ProdList
- 9891
- Advantage
- 58
- Tel
- Mobile:13665161512
- Fax
- +86-510-68873513
- Country
- China
- ProdList
- 1785
- Advantage
- 58
- Tel
- 025-85205967 13951876367
- Fax
- 025-85205967
- shengsaichem@163.com
- Country
- China
- ProdList
- 818
- Advantage
- 58
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 021-60345187 13671753212
- Fax
- 021-34702061
- lzz841106@aliyun.com
- Country
- China
- ProdList
- 10263
- Advantage
- 55
- Tel
- 19916721580
- Fax
- QQ：3154870176
- mafarm@126.com
- Country
- China
- ProdList
- 4542
- Advantage
- 58
View Lastest Price from 2-AMINO-4-IODOBENZOIC ACID manufacturers
- Product
- 2-AMINO-4-IODOBENZOIC ACID 20776-54-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2018-08-13