1H-Benzimidazole,5-chloro-2-ethyl-(9CI)

Product Name: 1H-Benzimidazole,5-chloro-2-ethyl-(9CI)
CAS No.: 34569-15-8
Chemical Name: 1H-Benzimidazole,5-chloro-2-ethyl-(9CI)
Synonyms: 6-chloro-2-ethyl-1H-Benzimidazole;1H-BenziMidazole, 6-chloro-2-ethyl-;5-chloro-2-ethyl-1H-benzo[d]imidazole;6-CHLORO-2-ETHYL-1H-BENZO[D]IMIDAZOLE;1H-Benzimidazole,5-chloro-2-ethyl-(9CI)
CBNumber: CB91283849
Molecular Formula: C9H9ClN2
Formula Weight: 180.63
MOL File: 34569-15-8.mol

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1H-Benzimidazole,5-chloro-2-ethyl-(9CI) Property

Melting point:: 168-170 °C
Boiling point:: 376.0±15.0 °C(Predicted)
Density: 1.291±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 10.59±0.10(Predicted)
Appearance: Light brown to brown Solid
InChI: InChI=1S/C9H9ClN2/c1-2-9-11-7-4-3-6(10)5-8(7)12-9/h3-5H,2H2,1H3,(H,11,12)
InChIKey: AIXMQUWDZVRMJJ-UHFFFAOYSA-N
SMILES: C1(CC)NC2=CC(Cl)=CC=C2N=1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR932774
Product name: 6-Chloro-2-ethyl-1H-benzimidazole
Purity: 95%
Packaging: 250mg
Price: $125
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-5-NB
Product name: 6-Chloro-2-ethyl-1H-benzimidazole
Purity: 95%
Packaging: 250mg
Price: $200
Updated: 2021/12/16

Apolloscientific

Product number: OR932774
Product name: 6-Chloro-2-ethyl-1H-benzimidazole
Purity: 95%
Packaging: 1g
Price: $225
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0124518
Product name: 1H-BENZIMIDAZOLE, 5-CHLORO-2-ETHYL-
Purity: 95.00%
Packaging: 5MG
Price: $499.28
Updated: 2021/12/16

Apolloscientific

Product number: OR932774
Product name: 6-Chloro-2-ethyl-1H-benzimidazole
Purity: 95%
Packaging: 5g
Price: $665
Updated: 2021/12/16

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1H-Benzimidazole,5-chloro-2-ethyl-(9CI) Chemical Properties,Usage,Production

Synthesis

95-83-0

7424-54-6

34569-15-8

4-Chloro-1,2-benzenediamine (71.0 mg, 0.5 mmol) and 3,5-heptanedione (64.0 mg, 0.5 mmol) were used as raw materials, and the above materials and p-toluenesulfonic acid (9.5 mg, 0.05 mmol) were added sequentially in a 25 mL Schlenk flask. Subsequently, toluene (4.0 mL) was added and the reaction mixture was placed in a 60°C oil bath and stirred for 24 hours. After completion of the reaction, the solvent was evaporated under reduced pressure. The crude product was separated by silica gel column chromatography using petroleum ether/ethyl acetate as eluent to afford 5-chloro-2-ethyl-1H-benzo[d]imidazole in 95% yield.

References

[1] Organic Letters, 2014, vol. 16, # 3, p. 764 - 767
[2] Patent: CN103910682, 2016, B. Location in patent: Paragraph 0035-0037
[3] Journal of Chemical Sciences, 2018, vol. 130, # 1,

1H-Benzimidazole,5-chloro-2-ethyl-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-Benzimidazole,5-chloro-2-ethyl-(9CI) Suppliers

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34569-15-8, 1H-Benzimidazole,5-chloro-2-ethyl-(9CI)Related Search:

1H-Benzimidazole,5-chloro-2-ethyl-(9CI)

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