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2-(2-Chloro ethoxy) Ethyl acetate

Product Name
2-(2-Chloro ethoxy) Ethyl acetate
CAS No.
14258-40-3
Chemical Name
2-(2-Chloro ethoxy) Ethyl acetate
Synonyms
ethyl 2-(2-chloroethoxy)acetate;NSC 72730;2-(2-Chloroethoxy)ethanol acetate;2-(2-chloroethoxy)-Ethanol 1-acetate;Ethanol,2-(2-chloroethoxy)-, 1-acetate
CBNumber
CB91465870
Molecular Formula
C6H11ClO3
Formula Weight
166.6
MOL File
14258-40-3.mol
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2-(2-Chloro ethoxy) Ethyl acetate Property

Boiling point:
223℃
Density 
1.119
Flash point:
92℃
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
InChI
InChI=1S/C6H11ClO3/c1-6(8)10-5-4-9-3-2-7/h2-5H2,1H3
InChIKey
ZUZWLUYOVJTJAG-UHFFFAOYSA-N
SMILES
C(OC(=O)C)COCCCl
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
HCH0362465
Product name
2-(2-CHLOROETHOXY)ETHYL ACETATE
Purity
95.00%
Packaging
5MG
Price
$502.47
Updated
2021/12/16
AHH
Product number
MT-29548
Product name
2-(2-chloroethoxy)ethanolacetate
Purity
98%
Packaging
25g
Price
$680
Updated
2021/12/16
Crysdot
Product number
CD41002002
Product name
2-(2-Chloroethoxy)ethylacetate
Purity
97%
Packaging
25g
Price
$120
Updated
2021/12/16
Crysdot
Product number
CD41002002
Product name
2-(2-Chloroethoxy)ethylacetate
Purity
97%
Packaging
100g
Price
$340
Updated
2021/12/16
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2-(2-Chloro ethoxy) Ethyl acetate Chemical Properties,Usage,Production

Synthesis

108-24-7

628-89-7

14258-40-3

To a stirred solution of 2-(2-chloroethoxy)ethan-1-ol (20.0 g, 160 mmol) in anhydrous dichloromethane (50 mL) was added triethylamine (Et3N, 33.4 mL, 176 mmol) and stirred at room temperature for 10 minutes. The reaction mixture was cooled to 0 °C and a dichloromethane (50 mL) solution of acetic anhydride (16.6 mL, 240 mmol) was added dropwise. Subsequently, the reaction mixture was warmed to room temperature and stirring was continued for 3 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was purified by column chromatography using 40% ethyl acetate/hexane as eluent to give 2-chloroethoxyethyl acetate. Yield: 17.5 g, 88%; 1H NMR (400 MHz, DMSO-d6) δ 4.12 (t, J = 4.5 Hz, 2H), 3.75-3.60 (m, 6H), 2.02 (s, 3H).

References

[1] Journal of Organic Chemistry, 2011, vol. 76, # 7, p. 2010 - 2028
[2] European Journal of Organic Chemistry, 2009, # 7, p. 1082 - 1092
[3] Patent: WO2018/98206, 2018, A1. Location in patent: Paragraph 0927
[4] ChemPlusChem, 2017, vol. 82, # 3, p. 423 - 432
[5] Patent: US2017/253569, 2017, A1. Location in patent: Paragraph 0990-0991

2-(2-Chloro ethoxy) Ethyl acetate Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(2-Chloro ethoxy) Ethyl acetate Suppliers

China 51 India 4 United Kingdom 2 United States 2 Global 59
Shanghai Qiao Chemical Science Co., Ltd
Tel
021-58892003
Email
info@qiaochem.com
Country
China
ProdList
6059
Advantage
65
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Beijing Isomersyn Technology CO;LTD
Tel
010-82954736 13391601435
Email
sales@isomersyn.com
Country
China
ProdList
3295
Advantage
57
Beijing Taiya Jie Technology Development Co., Ltd.
Tel
021-33690831-8001 13552411790
Fax
021-33690831
Email
postmaster@tyjchem.cn
Country
China
ProdList
1542
Advantage
55
Chengdu Ai Keda Chemical Technology Co., Ltd.
Tel
4008-755-333 18080918076
Fax
028-86757656
Email
800078821@qq.com
Country
China
ProdList
9718
Advantage
55
TIANJIN SPRING PHARMA SCIENCE CO., LTD.
Tel
0086-22-60330256
Fax
0086-22-60330256
Country
China
ProdList
83
Advantage
58
Shanghai Hao Yun Chemical Science Co.,Ltd.
Tel
021-68367562 15002147577;
Fax
021-68369562
Email
sales@haoyunchem.com
Country
China
ProdList
457
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55
HBCChem, Inc.
Tel
+1-510-219-6317
Fax
+1-650-486-1361
Email
sales@hbcchem.com
Country
United States
ProdList
10648
Advantage
60
Chengdu HuaXia Chemical Reagent Co. Ltd
Tel
400-1166-196 13458535857
Fax
QQ：800101999
Email
cdhxsj@163.com
Country
China
ProdList
13350
Advantage
58
Finetech Industry Limited
Tel
027-87465837 19945049750
Fax
027-8777-2287
Email
sales@finetechnology-ind.com
Country
China
ProdList
9637
Advantage
58
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View Lastest Price from 2-(2-Chloro ethoxy) Ethyl acetate manufacturers

Career Henan Chemica Co
Product
2-(2-Chloro ethoxy) Ethyl acetate 14258-40-3
Price
US $1.30/g
Min. Order
1g
Purity
98%
Supply Ability
1kg,10kg,100kg
Release date
2020-10-28

14258-40-3, 2-(2-Chloro ethoxy) Ethyl acetateRelated Search:


  • ethyl 2-(2-chloroethoxy)acetate
  • Ethanol,2-(2-chloroethoxy)-, 1-acetate
  • 2-(2-Chloroethoxy)ethanol acetate
  • NSC 72730
  • 2-(2-chloroethoxy)-Ethanol 1-acetate
  • 14258-40-3