2-(2-Chloro ethoxy) Ethyl acetate
- Product Name
- 2-(2-Chloro ethoxy) Ethyl acetate
- CAS No.
- 14258-40-3
- Chemical Name
- 2-(2-Chloro ethoxy) Ethyl acetate
- Synonyms
- ethyl 2-(2-chloroethoxy)acetate;NSC 72730;2-(2-Chloroethoxy)ethanol acetate;2-(2-chloroethoxy)-Ethanol 1-acetate;Ethanol,2-(2-chloroethoxy)-, 1-acetate
- CBNumber
- CB91465870
- Molecular Formula
- C6H11ClO3
- Formula Weight
- 166.6
- MOL File
- 14258-40-3.mol
2-(2-Chloro ethoxy) Ethyl acetate Property
- Boiling point:
- 223℃
- Density
- 1.119
- Flash point:
- 92℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- InChI
- InChI=1S/C6H11ClO3/c1-6(8)10-5-4-9-3-2-7/h2-5H2,1H3
- InChIKey
- ZUZWLUYOVJTJAG-UHFFFAOYSA-N
- SMILES
- C(OC(=O)C)COCCCl
N-Bromosuccinimide Price
- Product number
- HCH0362465
- Product name
- 2-(2-CHLOROETHOXY)ETHYL ACETATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.47
- Updated
- 2021/12/16
- Product number
- MT-29548
- Product name
- 2-(2-chloroethoxy)ethanolacetate
- Purity
- 98%
- Packaging
- 25g
- Price
- $680
- Updated
- 2021/12/16
- Product number
- CD41002002
- Product name
- 2-(2-Chloroethoxy)ethylacetate
- Purity
- 97%
- Packaging
- 25g
- Price
- $120
- Updated
- 2021/12/16
- Product number
- CD41002002
- Product name
- 2-(2-Chloroethoxy)ethylacetate
- Purity
- 97%
- Packaging
- 100g
- Price
- $340
- Updated
- 2021/12/16
2-(2-Chloro ethoxy) Ethyl acetate Chemical Properties,Usage,Production
Synthesis
108-24-7
628-89-7
14258-40-3
To a stirred solution of 2-(2-chloroethoxy)ethan-1-ol (20.0 g, 160 mmol) in anhydrous dichloromethane (50 mL) was added triethylamine (Et3N, 33.4 mL, 176 mmol) and stirred at room temperature for 10 minutes. The reaction mixture was cooled to 0 °C and a dichloromethane (50 mL) solution of acetic anhydride (16.6 mL, 240 mmol) was added dropwise. Subsequently, the reaction mixture was warmed to room temperature and stirring was continued for 3 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was purified by column chromatography using 40% ethyl acetate/hexane as eluent to give 2-chloroethoxyethyl acetate. Yield: 17.5 g, 88%; 1H NMR (400 MHz, DMSO-d6) δ 4.12 (t, J = 4.5 Hz, 2H), 3.75-3.60 (m, 6H), 2.02 (s, 3H).
References
[1] Journal of Organic Chemistry, 2011, vol. 76, # 7, p. 2010 - 2028
[2] European Journal of Organic Chemistry, 2009, # 7, p. 1082 - 1092
[3] Patent: WO2018/98206, 2018, A1. Location in patent: Paragraph 0927
[4] ChemPlusChem, 2017, vol. 82, # 3, p. 423 - 432
[5] Patent: US2017/253569, 2017, A1. Location in patent: Paragraph 0990-0991
2-(2-Chloro ethoxy) Ethyl acetate Preparation Products And Raw materials
Raw materials
Preparation Products
2-(2-Chloro ethoxy) Ethyl acetate Suppliers
- Tel
- +1-510-219-6317
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- +1-650-486-1361
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View Lastest Price from 2-(2-Chloro ethoxy) Ethyl acetate manufacturers
- Product
- 2-(2-Chloro ethoxy) Ethyl acetate 14258-40-3
- Price
- US $1.30/g
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 1kg,10kg,100kg
- Release date
- 2020-10-28