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4-bromo-4'-(pentyloxy)-1,1'-biphenyl

Product Name
4-bromo-4'-(pentyloxy)-1,1'-biphenyl
CAS No.
63619-51-2
Chemical Name
4-bromo-4'-(pentyloxy)-1,1'-biphenyl
Synonyms
4-Bromo-4'-(pentyloxy)biphenyl;4-bromo-4'-(pentyloxy)-1,1'-biphenyl;4-(4-n-Pentyloxyphenyl)-bromobenzene;1,1'-Biphenyl, 4-bromo-4'-(pentyloxy)-
CBNumber
CB91525554
Molecular Formula
C17H19BrO
Formula Weight
319.24
MOL File
63619-51-2.mol
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4-bromo-4'-(pentyloxy)-1,1'-biphenyl Property

Melting point:
132 °C(Solv: hexane (110-54-3))
Boiling point:
401.6±28.0 °C(Predicted)
Density 
1.223±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
1397CJ
Product name
4-Bromo-4'-(pentyloxy)-1,1'-biphenyl
Packaging
10g
Price
$170
Updated
2021/12/16
Alichem
Product number
63619512
Product name
4-Bromo-4'-(pentyloxy)-1,1'-biphenyl
Packaging
10g
Price
$180
Updated
2021/12/16
Chemenu
Product number
CM254247
Product name
4-Bromo-4''-(pentyloxy)-1,1''-biphenyl
Purity
95+%
Packaging
10g
Price
$184
Updated
2021/12/16
Chemenu
Product number
CM254247
Product name
4-Bromo-4''-(pentyloxy)-1,1''-biphenyl
Purity
95+%
Packaging
25g
Price
$337
Updated
2021/12/16
Crysdot
Product number
CD00002962
Product name
4-Bromo-4'-(pentyloxy)-1,1'-biphenyl
Purity
97%
Packaging
25g
Price
$356
Updated
2021/12/16
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4-bromo-4'-(pentyloxy)-1,1'-biphenyl Chemical Properties,Usage,Production

Synthesis

110-53-2

29558-77-8

63619-51-2

GENERAL STEPS: 4'-Bromo-[1,1'-biphenyl]-4-ol (3.5 g, 14.11 mmol), 1-bromopentane (3.75 g, 21.05 mmol) and anhydrous potassium carbonate (4.9 g, 35.28 mmol) were suspended in 2-butanone (25 mL) under nitrogen protection. The reaction mixture was heated to reflux and kept for 8 hours. After completion of the reaction, it was cooled to room temperature and diluted with dichloromethane (50 mL). The insoluble salt was removed by filtration and the organic phase was washed sequentially with distilled water (50 mL) and saturated saline (50 mL). The organic layer was dried over anhydrous sodium sulfate and filtered and concentrated under reduced pressure to about 15 mL. The residue was washed with cold hexane (0 °C) to afford 4-bromo-4'-(pentyloxy)biphenyl (4.6 g, 94.3% yield) as a white solid.

References

[1] European Journal of Medicinal Chemistry, 2012, vol. 50, p. 196 - 208
[2] Chemistry Letters, 2010, vol. 39, # 5, p. 513 - 515
[3] Bioorganic and Medicinal Chemistry Letters, 2008, vol. 18, # 4, p. 1474 - 1477
[4] Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000, vol. 339, p. 145 - 158
[5] Patent: US5948753, 1999, A

4-bromo-4'-(pentyloxy)-1,1'-biphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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4-bromo-4'-(pentyloxy)-1,1'-biphenyl Suppliers

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63619-51-2, 4-bromo-4'-(pentyloxy)-1,1'-biphenylRelated Search:

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  • 4-bromo-4'-(pentyloxy)-1,1'-biphenyl
  • 4-Bromo-4'-(pentyloxy)biphenyl
  • 4-(4-n-Pentyloxyphenyl)-bromobenzene
  • 1,1'-Biphenyl, 4-bromo-4'-(pentyloxy)-
  • 63619-51-2