ChemicalBook > CAS DataBase List > 4-amino-2-bromobenzonitrile

4-amino-2-bromobenzonitrile

Product Name
4-amino-2-bromobenzonitrile
CAS No.
53312-82-6
Chemical Name
4-amino-2-bromobenzonitrile
Synonyms
Bromo-4-amino-benzonitrile;4-amino-2-bromobenzonitrile;Benzonitrile, 4-amino-2-bromo-;4-Amino-2-bromobenzonitrile,95%
CBNumber
CB91559319
Molecular Formula
C7H5BrN2
Formula Weight
197.03
MOL File
53312-82-6.mol
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4-amino-2-bromobenzonitrile Property

Boiling point:
355.5±32.0 °C(Predicted)
Density 
1.68
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
0.65±0.10(Predicted)
form 
Powder
color 
Yellow
InChI
InChI=1S/C7H5BrN2/c8-7-3-6(10)2-1-5(7)4-9/h1-3H,10H2
InChIKey
OSYGPHDNNWRFJO-UHFFFAOYSA-N
SMILES
C(#N)C1=CC=C(N)C=C1Br
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Safety

Safety Statements 
24/25
TSCA 
y
HazardClass 
6.1
HazardClass 
IRRITANT
HS Code 
29269090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
A595183
Product name
4-Amino-2-bromobenzonitrile
Packaging
100mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA67883
Product name
4-Amino-2-bromobenzonitrile
Packaging
10g
Price
$54
Updated
2021/12/16
Matrix Scientific
Product number
066623
Product name
4-Amino-2-bromobenzonitrile
Purity
98%
Packaging
5g
Price
$19
Updated
2021/12/16
Matrix Scientific
Product number
066623
Product name
4-Amino-2-bromobenzonitrile
Purity
98%
Packaging
25g
Price
$29
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA67883
Product name
4-Amino-2-bromobenzonitrile
Packaging
50g
Price
$215
Updated
2021/12/16
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4-amino-2-bromobenzonitrile Chemical Properties,Usage,Production

Chemical Properties

off-white Crysstalline

Synthesis

1220099-39-7

53312-82-6

The general procedure for the synthesis of 2-bromo-4-aminobenzonitrile from the compound (CAS:1220099-39-7) was as follows: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) (2.90 g, 12.8 mmol) was added to a 25 (4.03 g, 12.8 mmol) solution of 2-bromo-4-aminobenzonitrile (2,3-DCBQ) (2.90 g, 12.8 mmol) in a mixture of dichloromethane (CH2Cl2, 85 mL) and water ( H2O, 43 mL) in a stirred solution and the reaction was carried out at room temperature. The reaction mixture was stirred for 3.5 hours and then filtered to remove the precipitated solid. The filtrate was added to saturated aqueous sodium bicarbonate (NaHCO3) and extracted with dichloromethane (CH2Cl2). The organic layer was dried over magnesium sulfate (MgSO4) and concentrated. The residue obtained was purified by silica gel column chromatography (eluent: hexane/ethyl acetate = 2/1) to give 26 (2.13 g, 10.8 mmol, 85% yield) as a white solid.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 5, p. 1712 - 1717
[2] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 4, p. 993 - 1005

4-amino-2-bromobenzonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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4-amino-2-bromobenzonitrile Suppliers

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View Lastest Price from 4-amino-2-bromobenzonitrile manufacturers

Honest Joy Holdings Limited
Product
4-Amino-2-bromobenzonitrile 53312-82-6
Price
US $0.00/KG
Min. Order
1KG
Purity
98.5%
Supply Ability
100 tons
Release date
2022-01-14
Zhuozhou Wenxi import and Export Co., Ltd
Product
4-amino-2-bromobenzonitrile 53312-82-6
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
4-amino-2-bromobenzonitrile 53312-82-6
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09

53312-82-6, 4-amino-2-bromobenzonitrileRelated Search:

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  • Benzonitrile, 4-amino-2-bromo-
  • 4-Amino-2-bromobenzonitrile,95%
  • 53312-82-6