ChemicalBook > CAS DataBase List > methyl 3-(3-bromophenyl)propanoate
methyl 3-(3-bromophenyl)propanoate
- Product Name
- methyl 3-(3-bromophenyl)propanoate
- CAS No.
- 151583-29-8
- Chemical Name
- methyl 3-(3-bromophenyl)propanoate
- Synonyms
- ethyl 3-(3-broMophenyl)propanoate;Methyl 3-(3-bromophenyl)propionate;methyl 3-(3-bromophenyl)propanoate;3-bromoBenzenepropanoic acid methyl ester;3-(3-Bromophenyl)propionic acid methyl ester;Benzenepropanoic acid, 3-broMo-, Methyl ester
- CBNumber
- CB91563916
- Molecular Formula
- C10H11BrO2
- Formula Weight
- 243.1
- MOL File
- 151583-29-8.mol
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methyl 3-(3-bromophenyl)propanoate Property
- Boiling point:
- 287.3±15.0 °C(Predicted)
- Density
- 1.382
- refractive index
- 1.540
- Flash point:
- >110℃
- storage temp.
- Sealed in dry,Room Temperature
- form
- liquid
- Appearance
- Colorless to light yellow Liquid
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Safety
- WGK Germany
- nwg
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 730165
- Product name
- Methyl 3-(3-bromophenyl)propionate
- Purity
- 97%
- Packaging
- 1g
- Price
- $58.5
- Updated
- 2023/01/07
TRC
- Product number
- M296170
- Product name
- Methyl3-(3-bromophenyl)propanoate
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
TRC
- Product number
- M296170
- Product name
- Methyl3-(3-bromophenyl)propanoate
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0369228
- Product name
- METHYL-3-(3-BROMOPHENYL)PROPANOATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $147
- Updated
- 2021/12/16
AK Scientific
- Product number
- W3312
- Product name
- Methyl3-(3-bromophenyl)propanoate
- Packaging
- 5g
- Price
- $235
- Updated
- 2021/12/16
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methyl 3-(3-bromophenyl)propanoate Chemical Properties,Usage,Production
Synthesis
67-56-1
23689-33-0
151583-29-8
GENERAL METHOD: An appropriate amount of bromophenyl streptanoic acid (1 equiv.) was dissolved in methanol (25 mL) and stirred to form a homogeneous solution. Sulfuric acid (0.1 equiv. concentration solution) was slowly added to this solution and the reaction mixture was subsequently heated to reflux and maintained for 18 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated under reduced pressure to remove the solvent. The concentrated oily product was diluted with saturated aqueous sodium bicarbonate solution (50 mL) and subsequently extracted with ether (3 x 25 mL). All ether extracts were combined, washed with brine (100 mL) and dried over anhydrous magnesium sulfate. After filtration to remove the desiccant, the filtrate was concentrated under reduced pressure to give the target product methyl 3-bromo-3-phenylpropionate.
References
[1] European Journal of Medicinal Chemistry, 2018, vol. 143, p. 1644 - 1656
methyl 3-(3-bromophenyl)propanoate Preparation Products And Raw materials
Raw materials
Preparation Products
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