ChemicalBook > CAS DataBase List > 1-TERT-BUTYL-4-NITROBENZENE

1-TERT-BUTYL-4-NITROBENZENE

Product Name
1-TERT-BUTYL-4-NITROBENZENE
CAS No.
3282-56-2
Chemical Name
1-TERT-BUTYL-4-NITROBENZENE
Synonyms
4-t-Butylnitrobenzene;p-t-Butylnitrobenzene;p-Nitro-t-butylbenzene;4-tert-Butylnitrobenzene;P-TERT-BUTYLNITROBENZENE;P-NITRO-TERT-BUTYLBENZENE;4-Nitro-tert-butylbenzene;1-TERT-BUTYL-4-NITROBENZENE;1-Nitro-4-tert-butylbenzene;1-tert-Butyl-4-nitrobenzene >
CBNumber
CB9164886
Molecular Formula
C10H13NO2
Formula Weight
179.22
MOL File
3282-56-2.mol
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1-TERT-BUTYL-4-NITROBENZENE Property

Melting point:
1°C (estimate)
Boiling point:
265-267°C
Density 
1,0586 g/cm3
refractive index 
1.5340
Flash point:
265-267°C
storage temp. 
Store at room temperature
form 
clear liquid
color 
Light yellow to Yellow to Orange
BRN 
2047337
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Safety

Safety Statements 
23-24/25
HS Code 
2904.20.4500
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H301Toxic if swalloed

H311Toxic in contact with skin

H332Harmful if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B2149
Product name
1-tert-Butyl-4-nitrobenzene
Purity
>97.0%(GC)
Packaging
5g
Price
$34
Updated
2025/07/31
TCI Chemical
Product number
B2149
Product name
1-tert-Butyl-4-nitrobenzene
Purity
>97.0%(GC)
Packaging
25g
Price
$129
Updated
2025/07/31
TRC
Product number
B810025
Product name
1-tert-Butyl-4-nitrobenzene
Packaging
100mg
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
120000
Product name
1-(tert-Butyl)-4-nitrobenzene
Purity
95+%
Packaging
1g
Price
$72
Updated
2021/12/16
Oakwood
Product number
330007
Product name
1-(tert-Butyl)-4-nitrobenzene
Packaging
5g
Price
$25
Updated
2021/12/16
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1-TERT-BUTYL-4-NITROBENZENE Chemical Properties,Usage,Production

Synthesis

35779-04-5

3282-56-2

GENERAL STEPS: Add 1-tert-butyl-4-iodobenzene (0.5 mmol), copper(II) trifluoromethanesulfonate (45 mg, 0.125 mmol), potassium nitrite (KNO2, 128 mg, 1.5 mmol), and anhydrous dimethylsulfoxide (DMSO, 0.6 mL) to an oven-dried pressure tube under nitrogen atmosphere. The pressure tube was sealed with a polytetrafluoroethylene screw cap with a microvalve and purged through nitrogen for 5 min to displace the air. The mixture was stirred at room temperature for 10 minutes and then gradually warmed to 130 °C and the reaction was maintained at this temperature for 48 hours. Upon completion of the reaction, the mixture was cooled to room temperature, washed with excess ice water and extracted with ethyl acetate (3 x 10 mL). The organic phases were combined, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography (Table 2, entries 1-18) or basic alumina column chromatography (Table 2, entries 19-23) using a mixture of ethyl acetate and hexanes as eluent to give 1-tert-butyl-4-nitrobenzene in good final yield.

Purification Methods

Recrystallise it three times by partially freezing a mixture of the mono-nitro isomers, then recrystallise it twice from MeOH and dry it in vacuo [Brown J Am Chem Soc 81 3232 1959]. [Beilstein 5 H 418, 5 I 203, 5 II 321, 5 III 943, 5 IV 1052.]

References

[1] Tetrahedron Letters, 2005, vol. 46, # 28, p. 4715 - 4717
[2] Tetrahedron Letters, 2012, vol. 53, # 12, p. 1511 - 1513

1-TERT-BUTYL-4-NITROBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-TERT-BUTYL-4-NITROBENZENE Suppliers

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View Lastest Price from 1-TERT-BUTYL-4-NITROBENZENE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
1-TERT-BUTYL-4-NITROBENZENE 3282-56-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-07-11

3282-56-2, 1-TERT-BUTYL-4-NITROBENZENERelated Search:

2-METHYL-2-(4-NITROPHENYL)-PROPIONIC ACID 1,1,3,3,5-PENTAMETHYL-4,6-DINITROINDANE 2,4,6-Tri-tert-butyl-1-nitrobenzene,1,3,5-TRI-TERT-BUTYL-2-NITROBENZENE Musk xylene 1-TERT-BUTYL-4-NITROBENZENE N-T-BUTYL 3-NITROBENZENESULFONAMIDE N-tert-Butyl 4-Nitrophenylsulfonamide 4-tert-Butyl-2-nitrophenyl propyl ether 4-TERT-BUTYL-2-NITROBENZENETHIOL 1-TERT-BUTYL-2-NITROBENZENE 97%,1-TERT-BUTYL-2-NITROBENZENE 3-(4-NITROPHENYL)ADAMANTANE-1-CARBOXYLIC ACID 2,6-DINITRO-3-TERT-BUTYL-4-ISOPROPYLTOLUENE 2-DIETHYLAMINOETHYL 1-(4-NITROPHENYL)CYCLOPENTANECARBOXYLATE HYDROCHLORIDE 1-(4-NITROPHENYL)CYCLOPENTANE-1-CARBOXYLICACID 2-methyl-2-(4-nitrophenyl)propanenitrile 4-bromo-2-tert-butyl-1-nitrobenzene 1-TERT-BUTYL-3-NITROBENZENE 2,6-ditert-butyl-3-nitroaniline

  • 4-t-Butylnitrobenzene
  • 4-tert-Butylnitrobenzene
  • Benzene, 1-(1,1-dimethylethyl)-4-nitro-
  • p-Nitro-t-butylbenzene
  • p-t-Butylnitrobenzene
  • P-TERT-BUTYLNITROBENZENE
  • P-NITRO-TERT-BUTYLBENZENE
  • 1-TERT-BUTYL-4-NITROBENZENE
  • 4-Nitro-tert-butylbenzene
  • 1-(1,1-Dimethylethyl)-4-nitrobenzene
  • 1-Nitro-4-tert-butylbenzene
  • 1-<i>tert</i>-Butyl-4-nitrobenzene
  • 1-tert-Butyl-4-nitrobenzene &gt
  • 3282-56-2