6-Bromo-5-fluoroindole

Product Name: 6-Bromo-5-fluoroindole
CAS No.: 259860-08-7
Chemical Name: 6-Bromo-5-fluoroindole
Synonyms: 6-Bromo-5-fluoroindole;6-Bromo-6-fluoroindole;6-bromo-5-fluoro-1H-indole;1H-Indole, 6-broMo-5-fluoro-
CBNumber: CB91876487
Molecular Formula: C8H5BrFN
Formula Weight: 214.03
MOL File: 259860-08-7.mol

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6-Bromo-5-fluoroindole Property

Melting point:: 82-84 °C
Boiling point:: 315.9±22.0 °C(Predicted)
Density: 1.750
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: solid
pka: 15.23±0.30(Predicted)
Appearance: Light yellow to brown Solid

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Safety

Hazard Codes: Xn
Risk Statements: 22-37/38-41
Safety Statements: 26-39
WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 691526
Product name: 6-Bromo-5-fluoroindole
Purity: 97%
Packaging: 1g
Price: $400
Updated: 2023/06/20

Sigma-Aldrich

Product number: 691526
Product name: 6-Bromo-5-fluoroindole
Purity: 97%
Packaging: 250mg
Price: $227
Updated: 2022/05/15

TRC

Product number: B686408
Product name: 6-Bromo-5-fluoro-1H-indole
Packaging: 500mg
Price: $175
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-3-0J
Product name: 6-Bromo-5-fluoro-1H-indole
Packaging: 1g
Price: $175
Updated: 2021/12/16

Matrix Scientific

Product number: 067078
Product name: 6-Bromo-5-fluoroindole
Purity: 97%
Packaging: 500mg
Price: $52
Updated: 2021/12/16

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6-Bromo-5-fluoroindole Chemical Properties,Usage,Production

Synthesis

1034894-73-9

259860-08-7

General procedure for the synthesis of 5-fluoro-6-bromoindole from the compound (CAS:1034894-73-9): enamine (1.89 g, 4.38 mmol) was dissolved in ethanol (35.0 mL). To this solution, iron powder (4.42 g, 79.0 mmol) and acetic acid (35.0 mL) were added, and the reaction mixture was stirred at 90 °C overnight. After completion of the reaction, the reaction mixture was filtered and the filtrate was concentrated. The residue was purified by column chromatography (eluent: ethyl acetate/hexane, 1:9, v/v) to afford 6-bromo-5-fluoro-1H-indole as a yellow solid (0.83 g, 89% yield).1H NMR (CDCl3, 400 MHz) δ: 6.52 (m, 1H), 7.27 (m, 1H), 7.38 (d, J = 9.3 Hz, 1H) 7.57 (d, J = 5.7 Hz, 1H), 8.18 (br.s, 1H).

References

[1] Patent: WO2008/77138, 2008, A1. Location in patent: Page/Page column 77
[2] Patent: US2004/224973, 2004, A1. Location in patent: Page 22

6-Bromo-5-fluoroindole Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Bromo-5-fluoroindole Suppliers

China 119 India 1 Switzerland 1 United Kingdom 1 United States 10 Global 132

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View Lastest Price from 6-Bromo-5-fluoroindole manufacturers

Career Henan Chemical Co

Product: 6-Bromo-5-fluoro-1H-indole 259860-08-7
Price: US $1.00/g
Min. Order: 1g
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-10

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6-Bromo-5-fluoroindole

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6-bromo-5-fluoro-1H-indole

6-Bromo-6-fluoroindole

259860-08-7

Boronic Acid

Heterocyclic Compounds

Halogenated Heterocycles

Heterocyclic Building Blocks

Indoles

IndolesBuilding Blocks