ChemicalBook > CAS DataBase List > 2-Amino-3-methoxyphenol

2-Amino-3-methoxyphenol

Product Name
2-Amino-3-methoxyphenol
CAS No.
40925-69-7
Chemical Name
2-Amino-3-methoxyphenol
Synonyms
2-Amino-3-methoxyphenol;Phenol, 2-amino-3-methoxy-;2-Amino-3-methoxyphenol hydrochloride
CBNumber
CB92256129
Molecular Formula
C7H9NO2
Formula Weight
139.15
MOL File
40925-69-7.mol
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2-Amino-3-methoxyphenol Property

Boiling point:
265.1±25.0 °C(Predicted)
Density 
1.219±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
9.38±0.10(Predicted)
Appearance
Off-white to brown Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A898618
Product name
2-Amino-3-methoxyphenol
Packaging
500mg
Price
$220
Updated
2021/12/16
TRC
Product number
A898618
Product name
2-Amino-3-methoxyphenol
Packaging
100mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141324
Product name
2-Amino-3-methoxyphenol
Packaging
100mg
Price
$80
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141324
Product name
2-Amino-3-methoxyphenol
Packaging
250mg
Price
$160
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA141324
Product name
2-Amino-3-methoxyphenol
Packaging
2g
Price
$600
Updated
2021/12/16
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2-Amino-3-methoxyphenol Chemical Properties,Usage,Production

Synthesis

3114-61-2

40925-69-7

General procedure for the synthesis of 2-amino-3-methoxyphenol from 3-methoxy-2-nitrophenol: To a stirred solution of 3-methoxy-2-nitrophenol (8.78 g, 51.9 mmol) in ethanol (250 mL) was added 10% palladium-carbon catalyst (1 g), and the reaction mixture was stirred for 2.5 hr at room temperature and hydrogen atmosphere (1 atm). Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad to remove the catalyst. The filtrate was concentrated in vacuum to afford 2-amino-3-methoxyphenol (7.09 g, 51.0 mmol, 98% yield) as a yellow solid. The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 3.85 (3H, s), 6.46 (1H, d, J = 7.9 Hz), 6.48 (1H, d, J = 7.9 Hz), 7.40 (1H, t, J = 7.9 Hz), 10.22 (1H, s).

References

[1] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 5, p. 1644 - 1658
[2] Patent: EP2168959, 2010, A1. Location in patent: Page/Page column 123

2-Amino-3-methoxyphenol Preparation Products And Raw materials

Raw materials

Preparation Products

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40925-69-7, 2-Amino-3-methoxyphenolRelated Search:


  • 2-Amino-3-methoxyphenol
  • 2-Amino-3-methoxyphenol hydrochloride
  • Phenol, 2-amino-3-methoxy-
  • 40925-69-7