4-Iodophenethyl alcohol
- Product Name
- 4-Iodophenethyl alcohol
- CAS No.
- 52914-23-5
- Chemical Name
- 4-Iodophenethyl alcohol
- Synonyms
- Brn 1933621;2-(4-Iodophenyl);4-Iodobenzeneethanol;4-IODO PHENYL ETHANOL;Benzeneethanol, 4-iodo-;4-Iodophenethyl alcohol;p-Iodophenethyl alcohol;4-Iodophenylethylalcohol;2-(4-iodophenyl)ethan-1-ol;Phenethyl alcohol, p-iodo-
- CBNumber
- CB92335978
- Molecular Formula
- C8H9IO
- Formula Weight
- 248.06
- MOL File
- 52914-23-5.mol
4-Iodophenethyl alcohol Property
- Melting point:
- 48-49℃
- Boiling point:
- 276℃
- Density
- 1.749
- Flash point:
- 121℃
- storage temp.
- 2-8°C(protect from light)
- pka
- 14.79±0.10(Predicted)
- Appearance
- Off-white to yellow Solid
Safety
- HS Code
- 2905190098
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I718968
- Product name
- 2-(4-Iodophenyl)ethanol
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CS-W004990
- Product name
- 2-(4-Iodophenyl)ethanol
- Purity
- 98.77%
- Packaging
- 5g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- CS-W004990
- Product name
- 2-(4-Iodophenyl)ethanol
- Purity
- 98.77%
- Packaging
- 10g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 074776
- Product name
- 4-Iodophenylethylalcohol
- Purity
- 95+%
- Packaging
- 5g
- Price
- $399
- Updated
- 2021/12/16
- Product number
- W6745
- Product name
- 4-Iodophenylethylalcohol
- Packaging
- 5g
- Price
- $185
- Updated
- 2021/12/16
4-Iodophenethyl alcohol Chemical Properties,Usage,Production
Synthesis
1798-06-7
52914-23-5
To a stirred solution of 2-(4-iodophenyl)acetic acid (2.00 g, 7.63 mmol) in tetrahydrofuran (150 mL) was slowly added borane-tetrahydrofuran complex (1.0 M solution of tetrahydrofuran, 7.63 mL, 7.63 mmol) at room temperature. The reaction mixture was stirred continuously for 6 hours at room temperature. Upon completion of the reaction, the reaction mixture was diluted with saturated sodium chloride solution and the pH was adjusted with aqueous sodium hydroxide solution to 13. Subsequently, extraction was carried out with ethyl acetate and the organic phases were combined and dried over anhydrous sodium sulfate. After filtration to remove the desiccant, the filtrate was concentrated under reduced pressure to give 4-iodophenylethanol (620 mg, 33% yield) as a light orange solid. The product could be used in subsequent reactions without further purification. The results of low resolution mass spectrometry (electrospray ionization, ESI) were as follows: calculated value (C8H9IO) 248.1; measured value 271.1 (M + Na)+.
References
[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 34, p. 7865 - 7869
[2] Journal of the American Chemical Society, 2001, vol. 123, # 9, p. 1828 - 1833
[3] Liebigs Annalen der Chemie, 1994, # 11, p. 1075 - 1092
[4] Patent: WO2006/102760, 2006, A1. Location in patent: Page/Page column 121
[5] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 5, p. 647 - 652
4-Iodophenethyl alcohol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Iodophenethyl alcohol manufacturers
- Product
- 4-Iodophenethyl alcohol 52914-23-5
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
- Product
- 4-Iodophenethyl alcohol 52914-23-5
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09
- Product
- 4-Iodophenethyl alcohol 52914-23-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-12-18