ChemicalBook > CAS DataBase List > 2-Chloro-N-phenyl-isonicotinamide

2-Chloro-N-phenyl-isonicotinamide

Product Name
2-Chloro-N-phenyl-isonicotinamide
CAS No.
80194-83-8
Chemical Name
2-Chloro-N-phenyl-isonicotinamide
Synonyms
2-chloroisonicotinanilide;2-Chloro-N-phenyl-isonicotimide;2-Chloro-N-phenyl-isonicotinamide;4-Pyridinecarboxamide, 2-chloro-N-phenyl-
CBNumber
CB92445682
Molecular Formula
C12H9ClN2O
Formula Weight
232.67
MOL File
80194-83-8.mol
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2-Chloro-N-phenyl-isonicotinamide Property

Boiling point:
310.5±27.0 °C(Predicted)
Density 
1.341±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
11.19±0.70(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
2510AC
Product name
2-Chloro-N-phenylisonicotinamide
Packaging
250mg
Price
$92
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0069800
Product name
2-CHLORO-N-PHENYLPYRIDINE-4-CARBOXAMIDE
Purity
95.00%
Packaging
1G
Price
$765.23
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0069800
Product name
2-CHLORO-N-PHENYLPYRIDINE-4-CARBOXAMIDE
Purity
95.00%
Packaging
2.5G
Price
$1065.66
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0069800
Product name
2-CHLORO-N-PHENYLPYRIDINE-4-CARBOXAMIDE
Purity
95.00%
Packaging
5G
Price
$1295.03
Updated
2021/12/16
Ambeed
Product number
A121197
Product name
2-Chloro-N-phenylisonicotinamide
Purity
97%
Packaging
250mg
Price
$11
Updated
2021/12/16
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2-Chloro-N-phenyl-isonicotinamide Chemical Properties,Usage,Production

Synthesis

65287-34-5

62-53-3

80194-83-8

General procedure for the synthesis of 2-chloro-N-phenylisonicotinamide: 2-chloroisonicotinoyl chloride (10 g, 56.8 mmol) was dissolved in 1,2-dichloroethane (100 mL) and cooled to 0 °C. A mixed solution of aniline (5.70 mL, 62.5 mmol) and N,N-diisopropylethylamine (DIPEA, 10.2 mL, 59.6 mmol) in 1,2-dichloroethane (10 mL) was added slowly over about 1 hour. The reaction mixture was stirred at 0 °C for 1 h, then warmed up to 95 °C and kept for 1 h. The reaction was carried out at 0 °C. Upon completion of the reaction, it was cooled to room temperature, the reaction was quenched by the addition of water (30 mL) and the mixture was filtered. The filtrate was extracted with dichloromethane (200 mL) and the organic phases were combined. The organic phase was dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The residue was recrystallized with methanol/water (1:10, 110 mL) to afford the target product 2-chloro-N-phenylisonicotinamide (12.12 g, 92% yield).LC-MS analysis: retention time (RT) = 0.87 min; electrospray ionization mass spectrometry (ES+) = 233.1.

References

[1] Patent: WO2005/40120, 2005, A1. Location in patent: Page/Page column 23
[2] Patent: WO2005/40165, 2005, A1. Location in patent: Page/Page column 22
[3] Patent: WO2005/40173, 2005, A1. Location in patent: Page/Page column 33-34
[4] Patent: WO2005/54243, 2005, A1. Location in patent: Page/Page column 24-25
[5] Patent: WO2005/54244, 2005, A2. Location in patent: Page/Page column 23

2-Chloro-N-phenyl-isonicotinamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Chloro-N-phenyl-isonicotinamide manufacturers

Career Henan Chemica Co
Product
2-Chloro-N-phenyl-isonicotinamide 80194-83-8
Price
US $1.00/g
Min. Order
1g
Purity
85.0-99.8%
Supply Ability
20ton
Release date
2020-10-28

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