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2-Amino-3-chlorobenzaldehyde

Product Name
2-Amino-3-chlorobenzaldehyde
CAS No.
397322-82-6
Chemical Name
2-Amino-3-chlorobenzaldehyde
Synonyms
2-Amino-3-chlorobenzaldehyde;Benzaldehyde, 2-amino-3-chloro-;2-Amino-3-chlorobenzaldehyde 98%;3-Chloroanthranilaldehyde, 2-Chloro-6-formylaniline
CBNumber
CB92471683
Molecular Formula
C7H6ClNO
Formula Weight
155.58
MOL File
397322-82-6.mol
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2-Amino-3-chlorobenzaldehyde Property

Melting point:
30-31 °C
Boiling point:
264.3±25.0 °C(Predicted)
Density 
1.348±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
-1.59±0.10(Predicted)
Appearance
Light yellow to yellow Solid
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
A619863
Product name
2-Amino-3-chlorobenzaldehyde
Packaging
100mg
Price
$265
Updated
2021/12/16
AK Scientific
Product number
9811DA
Product name
2-Amino-3-chlorobenzaldehyde
Packaging
100mg
Price
$116
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-5-20
Product name
2-Amino-3-chlorobenzaldehyde
Packaging
250mg
Price
$122
Updated
2021/12/16
AK Scientific
Product number
9811DA
Product name
2-Amino-3-chlorobenzaldehyde
Packaging
250mg
Price
$136
Updated
2021/12/16
AK Scientific
Product number
9811DA
Product name
2-Amino-3-chlorobenzaldehyde
Packaging
1g
Price
$239
Updated
2021/12/16
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2-Amino-3-chlorobenzaldehyde Chemical Properties,Usage,Production

Synthesis

61487-25-0

397322-82-6

GENERAL METHOD: (2-Amino-3-chlorophenyl)methanol (1.2 g, 7.61 mmol) was dissolved in dichloromethane (20 mL) and manganese dioxide (2.6 g, 30.1 mmol) was added. The reaction mixture was stirred at room temperature for 23 hours under argon protection. After completion of the reaction, the solid catalyst was removed by filtration and the filtrate was concentrated under reduced pressure. The residue was recrystallized by ethyl acetate to give 2-amino-3-chlorobenzaldehyde (1.0 g, 85% yield) as yellow needle-like crystals.

References

[1] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 19, p. 5810 - 5831

2-Amino-3-chlorobenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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397322-82-6, 2-Amino-3-chlorobenzaldehydeRelated Search:


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