2-Amino-3-iodonaphthalene
- Product Name
- 2-Amino-3-iodonaphthalene
- CAS No.
- 116632-14-5
- Chemical Name
- 2-Amino-3-iodonaphthalene
- Synonyms
- 3-iodonaphthalen-2-amine;3-Iodo-2-naphthalenamine;2-Naphthalenamine,3-iodo-;2-Amino-3-iodonaphthalene
- CBNumber
- CB92478293
- Molecular Formula
- C10H8IN
- Formula Weight
- 269.08
- MOL File
- 116632-14-5.mol
2-Amino-3-iodonaphthalene Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- White to yellow Solid
Safety
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
N-Bromosuccinimide Price
- Product number
- I737335
- Product name
- 3-Iodonaphthalen-2-amine
- Packaging
- 100mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- 041216
- Product name
- 2-Amino-3-iodonaphthalene
- Packaging
- 50mg
- Price
- $384
- Updated
- 2021/12/16
- Product number
- 9743AC
- Product name
- 2-Amino-3-iodonaphthalene
- Packaging
- 1g
- Price
- $672
- Updated
- 2021/12/16
- Product number
- HCH0043420
- Product name
- 2-AMINO-3-IODONAPHTHALENE
- Purity
- 95.00%
- Packaging
- 50MG
- Price
- $999.08
- Updated
- 2021/12/16
- Product number
- 116632145
- Product name
- 3-Iodonaphthalen-2-amine
- Packaging
- 1g
- Price
- $998
- Updated
- 2021/12/16
2-Amino-3-iodonaphthalene Chemical Properties,Usage,Production
Synthesis
102153-71-9
116632-14-5
In a 250 mL three-necked flask, under nitrogen atmosphere, 0.04 mol 2-iodo-3-nitronaphthalene (Intermediate 2-1) and 0.08 mol SnCl2 were added and dissolved in 100 mL of ethanol. The mixture was heated to reflux and reacted for 6 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) and the reaction was stopped after confirming the complete consumption of intermediate 2-1. The reaction solution was allowed to cool to room temperature and filtered. The filtrate was rotary evaporated under reduced pressure until no fraction evaporated. Finally, the intermediate 2-2 (3-iodonaphthalen-2-amine) was purified by neutral silica gel column chromatography and analyzed by high performance liquid chromatography (HPLC) with 99.1% purity and 75.9% yield.
References
[1] Tetrahedron Letters, 2000, vol. 41, # 16, p. 2781 - 2785
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: CN107868051, 2018, A. Location in patent: Paragraph 0104; 0106
2-Amino-3-iodonaphthalene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Amino-3-iodonaphthalene manufacturers
- Product
- 2-Amino-3-iodonaphthalene 116632-14-5
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-10-10
- Product
- 2-Amino-3-iodonaphthalene 116632-14-5
- Price
- US $2.00-5.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-13
- Product
- 3-iodonaphthalen-2-amine 116632-14-5
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-19