ChemicalBook > CAS DataBase List > 4-Methoxy-2-(trifluoromethoxy)benzaldehyde

4-Methoxy-2-(trifluoromethoxy)benzaldehyde

Product Name
4-Methoxy-2-(trifluoromethoxy)benzaldehyde
CAS No.
886503-52-2
Chemical Name
4-Methoxy-2-(trifluoromethoxy)benzaldehyde
Synonyms
4-ForMyl-3-(trifluoroMethoxy)anisole;2-Trifluoromethoxy-4-methoxybenzaldehyde;4-METHOXY-2-(TRIFLUOROMETHOXY)BENZALDEHYDE;Benzaldehyde, 4-methoxy-2-(trifluoromethoxy)-;4-Formyl-3-(trifluoromethoxy)anisole, 2-Formyl-5-methoxy-alpha,alpha,alpha-trifluoroanisole
CBNumber
CB92498729
Molecular Formula
C9H7F3O3
Formula Weight
220.15
MOL File
886503-52-2.mol
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4-Methoxy-2-(trifluoromethoxy)benzaldehyde Property

Boiling point:
254℃
Density 
1.330
Flash point:
104℃
refractive index 
1.4870
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
Light yellow to yellow Liquid
Sensitive 
Air Sensitive
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Safety

HS Code 
2912120000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
M271830
Product name
4-Methoxy-2-(trifluoromethoxy)benzaldehyde
Packaging
100mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
W9156
Product name
2-Trifluoromethoxy-4-methoxybenzaldehyde
Packaging
25g
Price
$784
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0044779
Product name
4-METHOXY-2-(TRIFLUOROMETHOXY)BENZALDEHYDE
Purity
95.00%
Packaging
5G
Price
$895.01
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0044779
Product name
4-METHOXY-2-(TRIFLUOROMETHOXY)BENZALDEHYDE
Purity
95.00%
Packaging
10G
Price
$1283.57
Updated
2021/12/16
SynQuest Laboratories
Product number
2615-3-50
Product name
4-Methoxy-2-(trifluoromethoxy)benzaldehyde
Packaging
10g
Price
$336
Updated
2021/12/16
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4-Methoxy-2-(trifluoromethoxy)benzaldehyde Chemical Properties,Usage,Production

Synthesis

A mixture of n-butyllithium (8 mL, 20 mmol, 1 equiv, 2.5 M hexane) in Et2O (12 mL) was cooled to -78 0 C. The mixture was then cooled to -78 0 C. The mixture was then cooled to -78 0 C. The mixture was then cooled to -78 0 C. The mixture was then cooled to -78 0 C. A solution of 1-bromo-2-methoxy-4-trifluoromethoxybenzene (20 mmol) in Et2O (20 mL) was added to it dropwise via cannula. after 15 min, DMF (1.7 mL, 22 mmol, 1.1 eq) was added in batches via syringe, and the reaction mixture was stirred for an additional 15 min, and then heated to 0C. The reaction was then quenched with 1 M H2SO4 (20 mL) and partitioned. The aqueous phase was extracted with Et2O (3x) and the combined organic phases were washed and dried (brine, Na2SO4), filtered and concentrated. The resulting solid was recrystallized from hexane to give the desired product 4-methoxy-2-trifluoromethoxybenzaldehyde.

4-Methoxy-2-(trifluoromethoxy)benzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Methoxy-2-(trifluoromethoxy)benzaldehyde Suppliers

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886503-52-2, 4-Methoxy-2-(trifluoromethoxy)benzaldehydeRelated Search:


  • 4-Formyl-3-(trifluoromethoxy)anisole, 2-Formyl-5-methoxy-alpha,alpha,alpha-trifluoroanisole
  • 2-Trifluoromethoxy-4-methoxybenzaldehyde
  • 4-ForMyl-3-(trifluoroMethoxy)anisole
  • Benzaldehyde, 4-methoxy-2-(trifluoromethoxy)-
  • 4-METHOXY-2-(TRIFLUOROMETHOXY)BENZALDEHYDE
  • 886503-52-2
  • Fluorine series