6-Bromo-3-methoxypyridine-2-carboxaldehyde

Product Name: 6-Bromo-3-methoxypyridine-2-carboxaldehyde
CAS No.: 945954-95-0
Chemical Name: 6-Bromo-3-methoxypyridine-2-carboxaldehyde
Synonyms: 6-BroMo-3-Methoxypicolinaldehyde;6-Bromo-3-methoxy-pyridine-2-carbaldehyde;6-BroMo-3-Methoxy-2-pyridinecarboxaldehyde;6-Bromo-3-methoxypyridine-2-carboxaldehyde;2-Pyridinecarboxaldehyde, 6-broMo-3-Methoxy-
CBNumber: CB92500598
Molecular Formula: C7H6BrNO2
Formula Weight: 216.03
MOL File: 945954-95-0.mol

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6-Bromo-3-methoxypyridine-2-carboxaldehyde Property

Boiling point:: 301.4±37.0 °C(Predicted)
Density: 1.606
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 0.47±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB141702
Product name: 6-Bromo-3-methoxypicolinaldehyde
Packaging: 25mg
Price: $53
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB141702
Product name: 6-Bromo-3-methoxypicolinaldehyde
Packaging: 50mg
Price: $93
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB141702
Product name: 6-Bromo-3-methoxypicolinaldehyde
Packaging: 250mg
Price: $325
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB141702
Product name: 6-Bromo-3-methoxypicolinaldehyde
Packaging: 100mg
Price: $162
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367758
Product name: 6-BROMO-3-METHOXYPICOLINALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $501.39
Updated: 2021/12/16

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6-Bromo-3-methoxypyridine-2-carboxaldehyde Chemical Properties,Usage,Production

Synthesis

945954-94-9

945954-95-0

4. To a solution of methyl 6-bromo-3-methoxypyridinecarboxylate (7.56 g) obtained in Step 3 in tetrahydrofuran (THF) (110 mL) was slowly added diisobutylaluminum hydride (DIBAL-H) (1.5 M toluene solution, 24.6 mL) at -78 °C. The reaction mixture was stirred at -78 °C for 1 hour. Subsequently, the reaction mixture was warmed to 0 °C and stirring was continued. Upon completion of the reaction, the reaction was quenched by adding saturated aqueous sodium potassium tartrate (Rochelle salt) to the mixture and extracted with ethyl acetate. The organic layers were combined, washed with saturated sodium chloride (brine) solution, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent gradient: 0→33% ethyl acetate/hexane) and crystallized from ethyl acetate/hexane mixed solvent to give 6-bromo-3-methoxypyridine-2-carboxaldehyde (5.36 g, 81% yield) as white crystals.

References

[1] Patent: WO2007/89031, 2007, A1. Location in patent: Page/Page column 85

6-Bromo-3-methoxypyridine-2-carboxaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Bromo-3-methoxypyridine-2-carboxaldehyde Suppliers

China 36 India 1 United Kingdom 1 United States 6 Global 44

JinYan Chemicals(ShangHai) Co.,Ltd.

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SHANGHAI FDC-CHEMICAL CO.,LTD

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View Lastest Price from 6-Bromo-3-methoxypyridine-2-carboxaldehyde manufacturers

Career Henan Chemical Co

Product: 6-Bromo-3-methoxypyridine-2-carboxaldehyde 945954-95-0
Price: US $3.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10kg
Release date: 2019-09-10

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6-Bromo-3-methoxy-pyridine-2-carbaldehyde

945954-95-0