7-bromo-1H-indene
- Product Name
- 7-bromo-1H-indene
- CAS No.
- 16657-07-1
- Chemical Name
- 7-bromo-1H-indene
- Synonyms
- 4-bromo-3H-indene;7-bromo-1H-indene;7-Bromoindene, 97%;1H-Indene, 7-bromo-;7-Bromo-1H-indene
- CBNumber
- CB92512777
- Molecular Formula
- C9H7Br
- Formula Weight
- 195.06
- MOL File
- 16657-07-1.mol
7-bromo-1H-indene Property
- Boiling point:
- 257.0±29.0 °C(Predicted)
- Density
- 1.453 g/mL at 25 °C
- refractive index
- 1.6078 (589.3 nm 25℃)
- Flash point:
- >110℃
- storage temp.
- 2-8°C
- form
- liquid
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 729728
- Product name
- 7-Bromo-1H-indene
- Packaging
- 1g
- Price
- $113.22
- Updated
- 2025/07/31
- Product number
- B686858
- Product name
- 7-Bromo-1H-indene
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B686858
- Product name
- 7-Bromo-1H-indene
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B686858
- Product name
- 7-Bromo-1H-indene
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 121223
- Product name
- 7-Bromo-1H-indene
- Purity
- 96%
- Packaging
- 1g
- Price
- $98
- Updated
- 2021/12/16
7-bromo-1H-indene Chemical Properties,Usage,Production
Synthesis
16657-10-6
16657-07-1
45738-35-0
Synthesis of 4-bromo-1H-inden(d): 4-bromo-2,3-dihydro-1H-inden-1-ol (150 g, 704 mmol, 1 equiv) was suspended in a mixture of concentrated sulfuric acid (250 mL) and water (1.25 L). The reaction mixture was heated to reflux overnight. After completion of the reaction, it was cooled to room temperature and extracted with dichloromethane (1.5 L). The organic layer was washed sequentially with saturated sodium bicarbonate solution (1.5 L), dried over anhydrous sodium sulfate, and concentrated under reduced pressure to remove the solvent. The crude product obtained was purified by silica gel column chromatography (800 g silica gel), using heptane as eluent, to give 4-bromo-1H-indene (95 g, yield 69%) as a light yellow oil.
References
[1] Patent: WO2015/95188, 2015, A1. Location in patent: Paragraph 00163
[2] Angewandte Chemie - International Edition, 2010, vol. 49, # 38, p. 6877 - 6880
[3] Patent: US9249239, 2016, B2. Location in patent: Page/Page column 51; 52
7-bromo-1H-indene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 7-bromo-1H-indene manufacturers
- Product
- 7-bromo-1H-indene 16657-07-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98% HPLC
- Supply Ability
- 10 tons
- Release date
- 2020-02-01