5-Bromo-2-(methylthio)benzo[d]thiazole

Product Name: 5-Bromo-2-(methylthio)benzo[d]thiazole
CAS No.: 203395-29-3
Chemical Name: 5-Bromo-2-(methylthio)benzo[d]thiazole
Synonyms: 5-Bromo-2-(methylthio)benzothiazole;5-Bromo-2-(methylthio)benzo[d]thiazole;Benzothiazole, 5-bromo-2-(methylthio)-;5-bromo-2-methylsulfanyl-1,3-benzothiazole
CBNumber: CB92513471
Molecular Formula: C8H6BrNS2
Formula Weight: 260.17
MOL File: 203395-29-3.mol

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5-Bromo-2-(methylthio)benzo[d]thiazole Property

Boiling point:: 358.5±34.0 °C(Predicted)
Density: 1.72±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 0.72±0.10(Predicted)
form: solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: V4201
Product name: 5-Bromo-2-(methylthio)benzothiazole
Packaging: 250mg
Price: $211
Updated: 2021/12/16

Matrix Scientific

Product number: 091251
Product name: 5-Bromo-2-(methylthio)benzo[d]thiazole
Purity: 95+%
Packaging: 250mg
Price: $257
Updated: 2021/12/16

Matrix Scientific

Product number: 091251
Product name: 5-Bromo-2-(methylthio)benzo[d]thiazole
Purity: 95+%
Packaging: 1g
Price: $454
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0198784
Product name: 5-BROMO-2-(METHYLTHIO)BENZOTHIAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $496.94
Updated: 2021/12/16

Matrix Scientific

Product number: 091251
Product name: 5-Bromo-2-(methylthio)benzo[d]thiazole
Purity: 95+%
Packaging: 5g
Price: $1323
Updated: 2021/12/16

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5-Bromo-2-(methylthio)benzo[d]thiazole Chemical Properties,Usage,Production

Synthesis

71216-20-1

74-88-4

203395-29-3

Step B: Synthesis of 5-bromo-2-(methylthio)benzo[d]thiazole; 5-bromobenzo[d]thiazole-2-thiol (24 mg, 0.098 mmol) was dissolved in ethanol (1.5 mL), and triethylamine (10 mg, 0.098 mmol) and iodomethane (14 mg, 0.098 mmol) were added sequentially. The reaction mixture was heated to reflux for 1.5 hours. After completion of the reaction, the reaction mixture was extracted with dichloromethane (3 x 10 mL). The organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford the target product 5-bromo-2-(methylthio)benzo[d]thiazole (20 mg, 80% yield).1H NMR (400 MHz, CDCl3) δ: 8.02 (s, 1H), 7.60 (d, 1H), 7.39 (d, 1H), 2.79 (s, 3H).

References

[1] Patent: WO2007/110364, 2007, A1. Location in patent: Page/Page column 57

5-Bromo-2-(methylthio)benzo[d]thiazole Preparation Products And Raw materials

Raw materials

Preparation Products

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203395-29-3, 5-Bromo-2-(methylthio)benzo[d]thiazoleRelated Search:

5-Bromo-2-(methylthio)benzo[d]thiazole

5-Bromo-2-(methylthio)benzothiazole

5-bromo-2-methylsulfanyl-1,3-benzothiazole

Benzothiazole, 5-bromo-2-(methylthio)-

203395-29-3