4-bromo-2-iodo-6-nitroaniline

Uses

Product Name: 4-bromo-2-iodo-6-nitroaniline
CAS No.: 180624-08-2
Chemical Name: 4-bromo-2-iodo-6-nitroaniline
Synonyms: 4-Bromo-2-iodo-7-nitroaniline;4-bromo-2-iodo-6-nitroaniline;4-BroMo-2-iodo-6-nitro-phenylaMine;Benzenamine, 4-bromo-2-iodo-6-nitro-;4-bromo-2-iodo-6-nitroaniline ISO 9001：2015 REACH
CBNumber: CB92525054
Molecular Formula: C6H4BrIN2O2
Formula Weight: 342.92
MOL File: 180624-08-2.mol

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4-bromo-2-iodo-6-nitroaniline Property

Melting point:: 146-147 °C
Boiling point:: 356.7±42.0 °C(Predicted)
Density: 2.418±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: -3.25±0.25(Predicted)
Appearance: Yellow to orange Solid

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 9471AA
Product name: 4-Bromo-2-iodo-6-nitroaniline
Packaging: 1g
Price: $184
Updated: 2021/12/16

Matrix Scientific

Product number: 089737
Product name: 4-Bromo-2-iodo-6-nitroaniline
Purity: 95+%
Packaging: 250mg
Price: $227
Updated: 2021/12/16

Apolloscientific

Product number: OR400643
Product name: 4-Bromo-2-iodo-6-nitroaniline
Packaging: 1g
Price: $319
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0365611
Product name: 4-BROMO-2-IODO-6-NITROANILINE
Purity: 95.00%
Packaging: 5MG
Price: $501.95
Updated: 2021/12/16

Matrix Scientific

Product number: 089737
Product name: 4-Bromo-2-iodo-6-nitroaniline
Purity: 95+%
Packaging: 1g
Price: $504
Updated: 2021/12/16

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4-bromo-2-iodo-6-nitroaniline Chemical Properties,Usage,Production

Uses

4-Bromo-2-iodo-6-nitroaniline is a useful research chemical compound.

Synthesis

875-51-4

180624-08-2

General procedure for the synthesis of 2-iodo-4-bromo-6-nitroaniline from 4-bromo-2-nitroaniline: 4-bromo-2-nitroaniline (14.3 g, 0.0659 mol) was added in a single addition to a solution of iodine (17.6 g, 0.0692 mol) dissolved in ethanol (300 mL), followed by the addition of silver (I) sulfate (20.4 g, 0.0659 mol). The reaction mixture was stirred at room temperature for 18 hours and then filtered. The resulting solid was washed with dichloromethane until all the orange product was dissolved. The filtrates were combined and the solid obtained after vacuum evaporation was washed with a solvent mixture of ether/40-60 petroleum ether (1:1) and filtered to give 4-bromo-2-iodo-6-nitroaniline as an orange solid (19.8 g, 88% yield), which could be used in the subsequent reaction without further purification.1H NMR (400 MHz, CDCl3, δ): 6.15 (2H, br s) 8.00 (1H, s), 8.42 (1H, s).

References

[1] Journal of Organic Chemistry, 1996, vol. 61, # 17, p. 5804 - 5812
[2] Patent: WO2007/148093, 2007, A1. Location in patent: Page/Page column 14-15
[3] Journal of Organic Chemistry, 2018, vol. 83, # 17, p. 10627 - 10635
[4] RSC Advances, 2018, vol. 8, # 54, p. 30761 - 30776
[5] Patent: WO2017/19828, 2017, A1. Location in patent: Page/Page column 57

4-bromo-2-iodo-6-nitroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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4-bromo-2-iodo-6-nitroaniline Suppliers

China 46 India 2 United Kingdom 1 United States 8 Global 57

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180624-08-2, 4-bromo-2-iodo-6-nitroanilineRelated Search:

4-BROMO-2-IODOPYRIDINE 4-Bromo-2-iodo-7-azaindole

4-bromo-2-iodo-6-nitroaniline

4-BroMo-2-iodo-6-nitro-phenylaMine

Benzenamine, 4-bromo-2-iodo-6-nitro-

4-bromo-2-iodo-6-nitroaniline ISO 9001：2015 REACH

4-Bromo-2-iodo-7-nitroaniline

180624-08-2