4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE

Product Name: 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE
CAS No.: 6296-89-5
Chemical Name: 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE
Synonyms: Methyl 4-hydrazinylbenzoate hydrochloride;AURORA 1803;methyl 4-hydrazinobenzoate hydrochloride;Dilarozil (Methylhydrazine Hydrochloride);4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE;Benzoic acid, 4-hydrazino-, Methyl ester, Monohydrochloride;Benzoic acid,4-hydrazinyl-, methyl ester, hydrochloride (1:1)
CBNumber: CB9256992
Molecular Formula: C8H11ClN2O2
Formula Weight: 202.64
MOL File: 6296-89-5.mol

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4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE Property

Melting point:: 205-207 °C
storage temp.: Inert atmosphere,Room Temperature
Appearance: Off-white to light brown Solid
InChI: InChI=1S/C8H10N2O2.ClH/c1-12-8(11)6-2-4-7(10-9)5-3-6;/h2-5,10H,9H2,1H3;1H
InChIKey: MXSGRGCOQOKOEH-UHFFFAOYSA-N
SMILES: C1(C(=O)OC)C=CC(NN)=CC=1.Cl

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M323483
Product name: Methyl4-hydrazinylbenzoatehydrochloride
Packaging: 100mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: J97803
Product name: Methyl4-hydrazinylbenzoatehydrochloride
Packaging: 1g
Price: $48
Updated: 2021/12/16

Ark Pharm

Product number: P000642831
Product name: Methyl 4-hydrazinylbenzoate hydrochloride
Purity: 97%
Packaging: 1g
Price: $77
Updated: 2021/12/16

Ark Pharm

Product number: P000642831
Product name: Methyl 4-hydrazinylbenzoate hydrochloride
Purity: 97%
Packaging: 5g
Price: $270
Updated: 2021/12/16

Ark Pharm

Product number: P000642831
Product name: Methyl 4-hydrazinylbenzoate hydrochloride
Purity: 97%
Packaging: 10g
Price: $385
Updated: 2021/12/16

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4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE Chemical Properties,Usage,Production

Uses

Methyl 4-hydrazinylbenzoate HCl

Synthesis

5326-27-2

6296-89-5

General procedure for the synthesis of methyl 4-hydrazinylbenzoate hydrochloride from 2-hydrazinylbenzoic acid: 4M dioxane solution of hydrogen chloride (100 mL, 399.60 mmol) was slowly added to a solution of 2-hydrazinylbenzoic acid (15.2 g, 99.90 mmol) in methanol (200 mL). The reaction mixture was stirred at 90 °C for 5 hours. Upon completion of the reaction, it was cooled to 20 °C and the resulting precipitate was collected by filtration, washed with ether (100 mL) and subsequently dried under vacuum to afford the target product methyl 4-hydrazinobenzoate hydrochloride (16.50 g, 82% yield) as a milky white crystalline solid. Mass spectrometry analysis (ESI-) showed m/z (M-H)- = 165; high performance liquid chromatography (HPLC) retention time was 1.12 min. 1H NMR (400.13 MHz, DMSO-d6) δ 3.81 (3H, s, OCH3), 6.99-7.02 (2H, m, Ar-H), 7.86-7.90 (2H, m, Ar- H), 8.98 (1H, s, NH), 10.47 (3H, s, NH3+).

References

[1] Patent: WO2008/99145, 2008, A1. Location in patent: Page/Page column 155-156
[2] Patent: WO2008/99145, 2008, A1. Location in patent: Page/Page column 156

4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE Suppliers

Austria 1 China 43 India 1 United States 4 Global 49

Chengdu Jiuding Chemical Technology Co., Ltd. - Song Bo

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View Lastest Price from 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE 6296-89-5
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 2000tons
Release date: 2025-08-22

6296-89-5, 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDERelated Search:

4-Hydrazinylbenzoic acid ETHYL 1-(5-CHLORO-1-[4-(ETHOXYCARBONYL)PHENYL]-6-OXO-1,6-DIHYDROPYRIDAZIN-4-YL)PIPERIDINE-4-CARBOXYLATE 4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL ETHYL 4-{(2E)-2-[3-(4-CHLOROPHENYL)-5-IMINO-1-METHYL-1,5-DIHYDRO-4H-PYRAZOL-4-YLIDENE]HYDRAZINO}BENZOATE ETHYL 4-(4,5-DICHLORO-6-OXO-1,6-DIHYDROPYRIDAZIN-1-YL)BENZOATE 4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE ETHYL 4-[5-CHLORO-4-(2,6-DIMETHYLMORPHOLINO)-6-OXOPYRIDAZIN-1(6H)-YL]BENZOATE ETHYL 4-[5-CHLORO-4-(DIETHYLAMINO)-6-OXOPYRIDAZIN-1(6H)-YL]BENZOATE ETHYL 4-[5-CHLORO-4-MORPHOLINO-6-OXOPYRIDAZIN-1(6H)-YL]BENZOATE methyl 4-(4,5-dichloro-6-oxopyridazin-1(6H)-yl)benzoate ETHYL 4-[(2E)-2-(1-CHLORO-2-ETHOXY-2-OXOETHYLIDENE)HYDRAZINO]BENZOATE 2,3-DICHLORO-4-(2-[4-(ETHOXYCARBONYL)PHENYL]HYDRAZONO)BUT-2-ENOIC ACID ETHYL 4-[(2E)-2-(1-CHLORO-2-OXOPROPYLIDENE)HYDRAZINO]BENZOATE

4-HYDRAZINOBENZOIC ACID METHYL ESTER HYDROCHLORIDE

AURORA 1803

Benzoic acid, 4-hydrazino-, Methyl ester, Monohydrochloride

Methyl 4-hydrazinylbenzoate hydrochloride

methyl 4-hydrazinobenzoate hydrochloride

Benzoic acid,4-hydrazinyl-, methyl ester, hydrochloride (1:1)

Dilarozil (Methylhydrazine Hydrochloride)

6296-89-5