2,6-dichloro-N-Methylpyridin-4-aMine

Product Name: 2,6-dichloro-N-Methylpyridin-4-aMine
CAS No.: 175461-33-3
Chemical Name: 2,6-dichloro-N-Methylpyridin-4-aMine
Synonyms: 2,6-dichloro-4-methylamino-pyridine;2,6-dichloro-N-methyl-4-Pyridinamine;2,6-dichloro-N-Methylpyridin-4-aMine;4-Pyridinamine, 2,6-dichloro-N-methyl-
CBNumber: CB92583038
Molecular Formula: C6H6Cl2N2
Formula Weight: 177.03
MOL File: 175461-33-3.mol

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2,6-dichloro-N-Methylpyridin-4-aMine Property

Melting point:: 70 °C
Boiling point:: 312.0±37.0 °C(Predicted)
Density: 1.404±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 0.79±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR948201
Product name: 2,6-Dichloro-N-methylpyridin-4-amine
Purity: 95%
Packaging: 1g
Price: $370
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0362943
Product name: 2,6-DICHLORO-N-METHYLPYRIDIN-4-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $495.81
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-5-AH
Product name: 2,6-Dichloro-N-methylpyridin-4-amine
Purity: 95%
Packaging: 1g
Price: $592
Updated: 2021/12/16

AK Scientific

Product number: 9193AA
Product name: 2,6-Dichloro-N-methylpyridin-4-amine
Packaging: 10g
Price: $784
Updated: 2021/12/16

Abosyn

Product number: 10-1576
Product name: (2,6-Dichloro-pyridin-4-yl)-methyl-amine
Purity: >95%
Packaging: 5g
Price: $870
Updated: 2021/12/16

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2,6-dichloro-N-Methylpyridin-4-aMine Chemical Properties,Usage,Production

Synthesis

16063-69-7

74-89-5

175461-33-3

GENERAL STEPS: 2,4,6-Trichloropyridine (20.0 g, 109.63 mmol) was dissolved in anhydrous ethanol (100 mL). An ethanol solution of 33% methylamine (81.9 mL, 657 mmol) was added slowly and dropwise at room temperature. The reaction mixture was stirred continuously at room temperature for 2 weeks. After completion of the reaction, the white precipitate was collected by filtration and washed with methyl tert-butyl ether and deionized water sequentially to afford 2,6-dichloro-4-methylaminopyridine (11.9 g, 61% yield) as white crystals.

References

[1] Patent: WO2008/92942, 2008, A2. Location in patent: Page/Page column 22
[2] Patent: WO2006/53166, 2006, A1. Location in patent: Page/Page column 57-58
[3] New Journal of Chemistry, 2016, vol. 40, # 11, p. 9194 - 9204
[4] Patent: WO2006/122137, 2006, A1. Location in patent: Page/Page column 71-72
[5] Patent: US2015/57260, 2015, A1. Location in patent: Paragraph 0300; 0331; 0551; 0552

2,6-dichloro-N-Methylpyridin-4-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-dichloro-N-Methylpyridin-4-aMine Suppliers

China 45 India 1 United States 5 Global 51

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175461-33-3, 2,6-dichloro-N-Methylpyridin-4-aMineRelated Search:

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2,6-dichloro-N-Methylpyridin-4-aMine

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2,6-dichloro-4-methylamino-pyridine

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175461-33-3