2,6-dichloro-N-Methylpyridin-4-aMine
- Product Name
- 2,6-dichloro-N-Methylpyridin-4-aMine
- CAS No.
- 175461-33-3
- Chemical Name
- 2,6-dichloro-N-Methylpyridin-4-aMine
- Synonyms
- 2,6-dichloro-4-methylamino-pyridine;2,6-dichloro-N-methyl-4-Pyridinamine;2,6-dichloro-N-Methylpyridin-4-aMine;4-Pyridinamine, 2,6-dichloro-N-methyl-
- CBNumber
- CB92583038
- Molecular Formula
- C6H6Cl2N2
- Formula Weight
- 177.03
- MOL File
- 175461-33-3.mol
2,6-dichloro-N-Methylpyridin-4-aMine Property
- Melting point:
- 70 °C
- Boiling point:
- 312.0±37.0 °C(Predicted)
- Density
- 1.404±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 0.79±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2933399990
N-Bromosuccinimide Price
- Product number
- OR948201
- Product name
- 2,6-Dichloro-N-methylpyridin-4-amine
- Purity
- 95%
- Packaging
- 1g
- Price
- $370
- Updated
- 2021/12/16
- Product number
- HCH0362943
- Product name
- 2,6-DICHLORO-N-METHYLPYRIDIN-4-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.81
- Updated
- 2021/12/16
- Product number
- 3H31-5-AH
- Product name
- 2,6-Dichloro-N-methylpyridin-4-amine
- Purity
- 95%
- Packaging
- 1g
- Price
- $592
- Updated
- 2021/12/16
- Product number
- 9193AA
- Product name
- 2,6-Dichloro-N-methylpyridin-4-amine
- Packaging
- 10g
- Price
- $784
- Updated
- 2021/12/16
- Product number
- A130367
- Product name
- 2,6-Dichloro-N-methylpyridin-4-amine
- Purity
- 97%
- Packaging
- 250mg
- Price
- $53
- Updated
- 2021/12/16
2,6-dichloro-N-Methylpyridin-4-aMine Chemical Properties,Usage,Production
Synthesis
16063-69-7
74-89-5
175461-33-3
GENERAL STEPS: 2,4,6-Trichloropyridine (20.0 g, 109.63 mmol) was dissolved in anhydrous ethanol (100 mL). An ethanol solution of 33% methylamine (81.9 mL, 657 mmol) was added slowly and dropwise at room temperature. The reaction mixture was stirred continuously at room temperature for 2 weeks. After completion of the reaction, the white precipitate was collected by filtration and washed with methyl tert-butyl ether and deionized water sequentially to afford 2,6-dichloro-4-methylaminopyridine (11.9 g, 61% yield) as white crystals.
References
[1] Patent: WO2008/92942, 2008, A2. Location in patent: Page/Page column 22
[2] Patent: WO2006/53166, 2006, A1. Location in patent: Page/Page column 57-58
[3] New Journal of Chemistry, 2016, vol. 40, # 11, p. 9194 - 9204
[4] Patent: WO2006/122137, 2006, A1. Location in patent: Page/Page column 71-72
[5] Patent: US2015/57260, 2015, A1. Location in patent: Paragraph 0300; 0331; 0551; 0552
2,6-dichloro-N-Methylpyridin-4-aMine Preparation Products And Raw materials
Raw materials
Preparation Products
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