2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene
Uses- Product Name
- 2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene
- CAS No.
- 169247-46-5
- Chemical Name
- 2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene
- Synonyms
- 2-(Benzyloxy)-5-bromobenzotrifluoride;Benzyl 4-bromo-2-(trifluoromethyl)phenyl ether;2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene;1-(Benzyloxy)-4-bromo-2-(trifluoromethyl)benzene;4-bromo-1-phenylmethoxy-2-(trifluoromethyl)benzene;Benzene, 4-bromo-1-(phenylmethoxy)-2-(trifluoromethyl)-
- CBNumber
- CB92604469
- Molecular Formula
- C14H10BrF3O
- Formula Weight
- 331.13
- MOL File
- 169247-46-5.mol
2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene Property
- Boiling point:
- 346.4±42.0 °C(Predicted)
- Density
- 1.479±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- Appearance
- Colorless to light yellow Solid
N-Bromosuccinimide Price
- Product number
- B291558
- Product name
- 1-(Benzyloxy)-4-bromo-2-(trifluoromethyl)benzene
- Packaging
- 500mg
- Price
- $145
- Updated
- 2021/12/16
- Product number
- B291558
- Product name
- 1-(Benzyloxy)-4-bromo-2-(trifluoromethyl)benzene
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- HCH0362128
- Product name
- 1-(BENZYLOXY)-4-BROMO-2-(TRIFLUOROMETHYL)BENZENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.87
- Updated
- 2021/12/16
- Product number
- 095954
- Product name
- 1-(Benzyloxy)-4-bromo-2-(trifluoromethyl)benzene
- Purity
- 95+%
- Packaging
- 5g
- Price
- $840
- Updated
- 2021/12/16
- Product number
- 8660AA
- Product name
- 1-(Benzyloxy)-4-bromo-2-(trifluoromethyl)benzene
- Packaging
- 1g
- Price
- $137
- Updated
- 2021/12/16
2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene Chemical Properties,Usage,Production
Uses
4-Bromo-2-trifluoromethylbenzyl ether is an ether organic compound that can be used as a pharmaceutical synthesis intermediate.
Synthesis
50824-04-9
100-44-7
169247-46-5
First, 8.47 g of 4-bromo-2-trifluoromethylphenol, 5.34 g of potassium carbonate, 4.49 g of benzyl chloride and 100 mL of N,N-dimethylformamide were added to a reaction vial, and the reaction was stirred under the cooling of an ice bath.After 24 h, the reaction mixture was poured into ice water and extracted three times with 50 mL of ether. The organic phases were combined, washed with 10% aqueous sodium hydroxide, dried over anhydrous magnesium sulfate and concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography to give 9.38 g of 4-bromo-2-trifluoromethyl-1-benzyloxybenzene in 81% yield.
References
[1] Patent: US5530015, 1996, A
2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene Preparation Products And Raw materials
Raw materials
Preparation Products
2-(benzyloxy)-5-broMo-1-trifluoroMethylbenzene Suppliers
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